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GCMS analysis results for unknown compounds, sample AE10202, May 2002

Machine-extracted title · confidence 95%

Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10202 on May 10, 2002.

NYC-WTC_000045020–000045044

Folder label: “GCMS X 4/30/02 A 5/8/02

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Scanned page image, NYC-WTC_000045036
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\10202.D Vial: 20 Acq On 9 May 2002 6:53 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 8 1,5-Naphthalenedithiole Concentration Rank 6

T. EstConc Area Relative to ISTD R.T. 22.58 0.39 ug/L 672980 Phenanthranene-dl0 22.96 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 72 2 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 5 3 1,2 - Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 r 0 4 Anthracene, 9-methyl- ___________ 192 C15H12 000779-02- 50 Abundance Scan 3319 (22.580 min): 10202.D (-3312) (-) m/z 192.10 10 . 00% 192

5000

42 54 70 | 82 96 il 118 \ 146 160 136 , J . ! . ■ i ■ - 1 ' । 1 1 ' ' i r ■ 22.20 22.40 22.60 22.80 23.00 A O-TT i । 1 I । I । t it । ] r r m-lrt i |‘f l‘i i । i f H T1 tl t "t i|illi|iiii|iiii|ii | I i I f | I f Ti | । 1 I I'i'i I I । । । ■ ] I । I rT I i [ I । m/z 191.10 20.10% m/z->____ 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80950: 1,5-Naphthalenedithiole 192

5000 ■ i 1 1 1 ' i 1 ■ 1 ' r1 1 1 ' I 1 1 ' 1 1 1 159 22.20 22.40 22.60 22.80 23.00 115 128 m/z 146.10 14.75% 40 57 69 79 96 147 177 0 111111111111111111 i'i । ) । |'i i'i'i । i'i । lrvpprterrpa i'l1 -- "‘A" ■rrpm m/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192

22.20 22.40 22.60 22.80 23.00 5000 m/z 193.10 13.78%

69 90 108 122 134 m/z-> 45 0 .............................................. ii ,, 4 < I I ! | I < ‘ I | I ! I ! | I I I l‘| I I

0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 | 148 160 I''1 T " ‘ " 1' I 'i'1' Ir" T " 1 T "11' I I I I I I I I I I L I I I [ I 1 ( I I I Abundance #80862:1,2-Phenylene diisothiocyanate 192 22.20 22.40 22.60 22.80 23.00 m/z 96.10 11.49% 64 5000

39 50 75 90 134

0 ‘' r11 18| i I 28, 4 I [ r lit I 'I | I -tr ’rlj l'|TI107 122 , > 11 I ' h |'I ' I I | I 148 160 i "111'"' 11' " r1" i1"11 TI । । ■ > i । I ■ m/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 22.20 22.40 22.60 22.80 23.00

10202.D 050102.M Thu May 09 13:37:32 2002 Page 12

NYC-WTC_000045036

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NYC-WTC_000045036Source: NYC Law Department, mirrored locally

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