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GCMS analysis results for unknown compounds, sample AE10202, May 2002

Machine-extracted title · confidence 95%

Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10202 on May 10, 2002.

NYC-WTC_000045020–000045044

Folder label: “GCMS X 4/30/02 A 5/8/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\10202.D Vial: 20 Acq On 9 May 2002 6:53 am Operator: Mclean Sample 4/30 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 9 Phenanthrene-dlO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. •23.11 0.68 ug/L 1170610 Phenanthranene-dl0 22.96

Hit# of5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 86 2 Anthracene-a30- 188 C14D10 001719-06-8 72 3 Cycloheptanone, 4-phenyl - 188 C13H160 067688-28-2 50 4 Pentacyclo [7.3 . X1. (4,12) . 0 (2,7) . . . 188 C14H20 1000215-61-8 39 Abundance Scan 3409 (23.109 min): 10202.D (-3402) (-) m/z 188.10 100.00%! 188

5000

i । । r — 11 । m । । । । । । । । । ।—। r 80 94 42 54 66 . 122 132 146 158 1 22.80 23.00 23.20 23.40 o < 11 > > 111 p 1111 117'1 i ! । H'l 'i | T'f'ri"| iill1 + -HH | I > i > | f INy I ( I | I I I ! ] I I I I'|'l I I I J I I ! I | Il’r I" " i m/z 189.10 18.43%| m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 22.80 23.00 23.20 23.40 80 m/z 94.05 17,43%| 94 160 30 42 52 66 11 108 118 132 146 | 170179 0 l| | i । । i | i > iT| I > । i | I I i 1-| I I । i | । I I I | । I I I T1 I 1 I I i I | I I r I | i । i I । I i i i | I I I i । i I | I | 'I I' 111 |11 ri | | TII | |'PI PI | 7'I I

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

22.80 23.00 23.20 23.40 5000 m/z 80.10 14.42%

AS 80 94 160 , 17 30 42 52 0 J J 108 118 132 146 1 170179, | 0 । । । । । । । i । ■ i । ■ ■ । i | I i । i । I I । i । । I I Q 1 I I I | I i t I | I I । i | I i | I | i i I I | I i i r| I I I i । | i | i । 'i*t r'Pp r i । । i i i । | I'l l | | r I । T m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79739: Cycloheptanone, 4-phenyl- ........ /......................... Fl I I I I I J I I“ I I I I I" I I" I ' I I I "I 188 22.80 23.00 23.20 23.40 117 104 m/z 184.05 11.57% 91 160 5000 131 170 27 3 51 65 78 145

0 11 ‘ ' i1 ■, 1 111 h , I n I lhppel n n pmttmn , . 1 . . < IYI i-r I | I I I - I I I I I /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10202.D 050102.M Thu May 09 13:37:32 2002 Page 13

NYC-WTC_000045037

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NYC-WTC_000045037Source: NYC Law Department, mirrored locally

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