GCMS reference analysis results for sample AE06337, May 3 2002

Machine-extracted title · confidence 100%

Reference analysis report for GCMS testing of volatile organic compounds with quantified concentrations recorded on May 3 2002.

NYC-WTC_000044478–000044495

Folder label: “GCMS X 4/29/02 A 5/1/02”

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050102\6337.D Vial: 13 Acq On 1 May 2002 7:29 pm Operator: Mclean Sample re-ext 4/29 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.78 ug/L 811209 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO 188 C14D10 001517-22-2 90 2 Anthracene-dlO- 188 C14D10 001719-06-8 86 3 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 40 4 2-Quinolinecarboxaldehyde , 8-hyd... 188 C10H8N2O2 005603-22-5 38 Abundance Scan 3409 (23.109 min): 6337. D (-3403) (-) m/z 188.15 100.00% 188

5000

80 94 1 T 1111 TII))W I I I I I I I I I

22.80 23.00 23.20 23.40 42 54 66 1 । । । । । । i । । । I । । lii f —r । 146 160 । ■ ■ ■ ■ । ‘■ I j 1 ■ ' 1 "" | 253 ■ 1 i 1 1 1 ■ i 1 1 ■ ' i 1 1 '' 1 i m/ z 8.0.10 18.39% m/z->20 40 60 80) 100 120 140 160 180 200 220 240 Abundance #79827: Phenanthrene-d10 188

5000 1 1 i 1 1 7 1 I 1 1 1 ' I 1 1 '' I 22.80 23.00 23.20 23.40 m/ z 94.10 17.44% 80 94 160 | Il .108120132 146 dl... "..... 28 40 52 66 . I I I I I I r I I I I “ I I I I I I I 1 i pg 15378 । । ।' i i । i i । r । । । । i । i r । । । । i r 1 I ' ' ’ ' I ' ' ' ‘ I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #79826: Anthracene-d10- 188 1 1 I ' 1 III I I I I I-“I I I I 22.80 23.00 23.20 23.40 5000 m/z 189.10 15.64%

80 94 160 28 40 52 66 „l 196118,132-146— — - ■ ■ ■ । ■ ■ ■ ■ । ■ +‘r— - m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #79739: Cycloheptanone, 4-phenyl- ,p 1 1 l 188 22.80 23.00 23.20 23.40 117 m/ z 184.10 13.91% 104 91 160 5000 131

27 39 51 65 78 145

n/z-> Ji ,! lii hs, ik 1. ...Ill .1. - 1111111111 ii [iri111

20 40 60 80 100 ) 4140X i160 173 120 v 1 1 | ’ 180 200 220 240 I ■ I I I 1 I I I 1T°m 22.80 23.00 23.20 23.40 I I i I I —I I —

6337.D 050102.M Thu May 02 12:22:27 2002 Page 10

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