GCMS analysis results, sample AE09973, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050602\9973.D Vial : 21 Acq On 7 May 2002 3:59 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 15 Phenanthrene-dlO Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 23.11 0.54 ug/L 538533 Phenanthranene-dl0 22.96 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO 188 C14D10 001517-22-2 87 2 Anthracene-dl0- 188 C14D10 001719-06-8 83 3 2-Quinolinecarboxaldehyde , 8-hyd... 188 C10H8N2O2 005603-22-5 40 4 3-Amino-4-methyl -6-methoxyquinoline 188 C11H12N2O 1000213-71-3 38 Abundance Scan 3409 (23.109 min): 9973.D (-3403) (-) m/z 188.15 100.00% 188

5000

80 94 22.80 23.00 23.20 23.40 40 57 66 ITT IT r । । ii r । । । If ] 'i । । । । < I’ii । C3 . | i I i | | r I I .1 132 146 158 t i I i | 1 I i I | i I I t I I > I I I I I I I I I I I I I I I I I I rrI" I m/ z 80.10 19.46% II’I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 22.80 23.00 23.20 23.40 m/z 189.10 15.86% 80 94 160 30 42 52 66 . ,i| 108 118 132 146 I 170179.1,1 | ' I | I i । I | | | । | | r | • I | I I I i | I I | | | | lfvjvrlk It I | I I i i | I > i I । > i i i | । I I i pH f i । i i t i । i i'lll|li r । i | rrrrttlii iiii m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 > . । . .s < Yi । । । । । । । । । । । 22.80 23.00 23.20 23.40 5000 m/z 94.05 14.22%

as 80 94 160 1 17 30 42 52 0 J 108118 132 146 1 170179 '। । । ' । । ] । । । > j > i । । । I i । । । I I । । । I i I • । । । ! I | I । । I | I l r । | । I । I । । । । । । i । 1 i j H ! i ] i i 1 i [ । i |‘I'j'i i 1 1 । r ri i | 11111 Wr m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 1 I I I I I y I - I I I I _ I 1 I I I I" Abundance #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188 22.80 23.00 23.20 23.40 m/z 184.05 12.44%

5000 143 . 89 115

m/z-> ...... ... 51.64.76 11 02 130. 158 170 I | I T > t | I I I I | I I I I | ■ I > ' | । I I I | I I I I | I I I I | I I I I | I ' I I | I I I f | r I । I | I I I I | I I I

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 If I I | I I I I [ I I I I I I I I I I I I I1 Wr ' 1 I ' 1 1 1 ' ' 1 1 1 ‘ * 1 I 22.80 23.00 23.20 23.40

9973.D 050102.M Tue May 07 15:52:03 2002 Page 19

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