GCMS analysis results for sample AE10303, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050802\10303.D Vial: 6 Acq On 8 May 2002 5:53 pm Operator: Mclean Sample 5/1 eh Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 23.11 0.52 ug/L 622430 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual 001517-22-2 83-/ 1 Phenanthrene-diO 188 C14D10 2 Anthracene-dlO- 188 C14D10 001719-06-8 72/ 3 3-Amino-4-methyl -6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 4 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 38 Abundance Scan 3409 (23.109 min): 10303.D (-3403) (-) m/z 188.10 100.00% 188

5000

80 94 1 1 । 1 ■ ' 1 i 1 ■ ' 1 i 1 '

160 22.80 23.00 23.20 23.40 132 1A 19 66 43 52 ‘, | I | I | | | | ( I1-.-I r . j I l . , । i . 14b |[| , ul l, 0 11" 111" 111 ■1'11 ■ " ■ i1'1 1111111111111111111111111 rl l| 1111111 1111111 m/z80.10 16.88% mlz-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 00/ 22.80 23.00 23.20 23.40 m/z 184.10 15.82% 30 42 52 66 80 94 11 108 118 132 146 160 ,i I 170179 ft 0 ’i [ । । i i [ । । 11 । । r t ri 11 I 11 । ] r I 11 । । i II i 11 f | I I । I | I I I I [ r I I I | I I I I | I I I I | I । I । | I rlT|*l I I I [ I I I J | I I I I | ITT TT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 . — ‘ 1 I 1 ,== I 22.80 23.00 23.20 23.40 5000 m/z 94.05 13.70%

94 80 ft 66 160 17 30 42 52 108 118 132 146 , J 170179 । 0 11" '11" H l " “ 11" ' i11 114i 11111 11111 TTtHm । 1111 11111 1111 I'lp 111111 1111’l’l Wr mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline ..................... 1 > | । i J । | i t.......................... r | i i i i ] i i i i [ 188 22.80 23.00 23.20 23.40 m/z 160.05 9.11% 145 5000

117 41 51 63 77 89 102 130 । 159 173 0 TT -Hrllr-ri rili’n । , I’’ . i ri1!1! I,, ’II np rll- , , rl-- , , H - 11..... rl 11'111 . — mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10303.D 050102.M Thu May 09 13:49:51 2002 Page 9

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