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GCMS analysis results for sample AE10308, May 2002

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10308 conducted on May 17, 2002.

NYC-WTC_000045171–000045188

Folder label: “GCMS X 5/1/02 A 5/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050802\10308.D Vial: 11 Acq On 8 May 2002 9:56 pm Operator: Mclean Sample 5/1 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************** Peak Number 6 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 23.11 0.59 ug/L 663994 Phenanthranene-d10 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual 'I 1 Anthracene-dlO- 188 C14D10 001719-06-8 72 2 Phenanthrene-diO 188 C14D10 001517-22-2 64 ' 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 50 4 Antipyrine 188 C11H12N2O 000060-80-0 40 Abundance Scan 3409 (23.109 min): 10308.D (-3403) (-) m/z 188.10 100.00% 188

5000 - 94 . F 80 158 22.80 23.00 23.20 23.40 =2 66 m/z-> 0 40 TTTT . + 132 -T I “ ‘' I 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 94.00 ft 20.91% Abundance #79826: Anthracene-d10- 188

5000 ‘ ' I ' ' ' ' I 1 1-1 1 I ov • i | > i > T-f 22.80 23.00 23.20 23.40 m/ z 189.10 15.65% 80 94 160 66 17 30 42 52 0 mCTHtt-H+ TTmn"uTDTTttr 108 118 132 146—41791794) nfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 .... 1................ ■ ■ i ■ ■ ■ ■ i > ■ - i > 1 । ।■ । । t—r

22.80 23.00 23.20 23.40 5000 m/z 184.15 13.28%

80 94 160 30 42 52 66 0 11 108118 132 I | I I J I | I J I I | I I I I [t 1 ! I ] I I I ! | 146.170179/ I,... m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 22.80 23.00 23.20 23.40 m/z 79.95 11.49% 145 5000

117 41 51 63 77 89 102 130 159 173 । I.... ■it/ i I I । I I ) । | I , J .............................................. O-r u 11111111■ -+-+#+++++-7--#l---+++-+---4---4-#7l4. 11’441 Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10308.D 050102.M Thu May 09 13:52:31 2002 Page 9

NYC-WTC_000045184

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NYC-WTC_000045184Source: NYC Law Department, mirrored locally

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