GCMS analysis results for sample AE10308, May 2002

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Data File : C:\MSDCHEM\1\DATA\050802\10308.D Vial: 11 Acq On : 8 May 2002 9:56 pm Operator: Mclean Sample : 5/1 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 4-Amino-4-cyano-1,3-dimethy... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 31.06 0.24 ug/L 225928 Chrysene-dl2 30.80 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-Amino-4-cyano-l,3-dimethyl-6-p... 229 C14H19N3 1000216-11-2 2 6-Amino-2-(m-tolyl)-1,3,5-thiadi... 235 C10H9N3S2 094014-50-3 3 8,8-Dimethyl-5,8,9,11-tetrahydro... 238 C13H18S2 1000210-31-7 5 4 cis-2H-Pyran, Tetrahydro-2,6-dip... 238 C17H180 055696-67- 5 Abundance Scan 4763 (31.065 min): 10308.D (-4761) (-) m/z 118.30 10 . 00% 104 1 8 235 A

207 5000 44

30.80 31.00 31.20 31.40 O+ ................. ........ ............ .Ui, , m/z 116.00 98.46% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 A Abundance #53851:4-Amino-4-cyano-1,3-dimethyl-6-phenylpiperidine 42 120 104

5000 70 158 91 30.80 31.00 31.20 31.40 55 132 202 m/z 235.00 87.18% 144 170 187 1 II 213 229 O+ ..... Ill 4lu—a— ILl.l, 1 4 lip j t, l pime. ’ I 1 11 1 1 1 1 mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #53046: 6-Amino-2-(m-tolyl)-1,3,5-thiadiazine-4-thione 1- 8

235 30.80 31.00 31.20 31.40 5000 m/ z 103.80 86.67% 91 43 65 143 I | । lu 1 ।, 77, । 177 202 220 / " I ' 1 i, OtIT 1 1441 ‘ 11 miz-> :20 40 60 80 100 120 140 160 180 200 220 240 Abundance #45104: 8,8-Dimethyl-5,8,9,11-tetrahydro-7H-6,10-dithiaben... 104 30.80 31.00 31.20 31.40 135 m/z 120.05 67.69%

5000 238 69 29 41 55 -, 91 117 |, 149 168 191 0 ----- " । । । ■ 1 ■ ■ । ■ I • ' i * ' i > । । i TT m/z-> 20 40 60 801 100 120 140 160 180 200 220 240 30.80 31.00 31.20 31.40

10308.D 050102.M Thu May 09 13:52:31 2002 Page 10

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