GCMS analysis results for sample AE10308, May 2002

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Data File C:\MSDCHEM\1\DATA\050802\10308.D Vial: 11 Acq On 8 May 2002 9:56 pm Operator: Mclean Sample 5/1 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Phenol, 3-chloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

34.90 0.66 ug/L 433920 Perylene-dl2 34.70 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Phenol, 3-chloro- 128 C6H5C10 000108-43-0 9/ 2 Parachlorophenol 128 C6H5C10 000106-48-9 8 3 Phenol, 2-chloro- 128 C6H5C10 000095-57-8 9 4 4-Amino-2-chloropyridine 128 C5H5C1N2 014432-12/3 9 Abundance Scan 5416 (34.901 min): 10308.D (-5415) (-) m/z 128.10 100.00% 128 fl /

5000 86 256 . — । । |--i । । । । 115 209 232 281 34.60 34.80 35.00 35.20

m/z-> 0- 49 ———— 1'111'1 'i1 ■111'1111 ........ I i 1 1 r 1 i ' 1 ' i 1 1 20 40 60 80 100 120 140 160 180 200 220 240 260 280 —1 m/z 129.40 85.27%

Abundance #57955: Phenol, 3-chloro- 128

A 5000 1 1 1 11 65 34.60 34.80 35.00 35.20 39 100 m/ Z 118.00 73.64%

0- , 12 26,+5241 +8744113— , 146 1 1 I ‘ ' 1 ' I ' ' ‘ 1 I 1 1 ‘ ' I ' ' ' 1 I 1 ' ' 1 I ' 1 ' ‘ I 1 1 1 ‘ I 1 1 mtz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #57956: Parachlorophenol 128

34.60 34.80 35.00 35.20 5000- 65 m/z 86.00 46.12% 39 100 26 - O—TTT 4441+524 +79 m/z—> 20 40 60 80) 100 120 140 160 180 200 220 240 260 280 Abundance #121753: Phenol, 2-chloro- A J AM Al WM AA , MAA AAAA A | 128 34.60 34.80 35.00 35.20 m/z 256.20 44.96% 5000 64

92 39 m/z—> 0 18 TIT ri dl ’r 20 40 60 +77108. ‘ I’’’’ r° *11 * 80 100 120 140 160 180 200 220 240 260 280 i 1 1 ' 1 i t ■ ■ ■ ■ i - ■ ■ ■ i ■ ■ 34.60 34.80 35.00 35.20

10308.D 050102.M Thu May 09 13:52:32 2002 Page 11

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