GCMS reference analysis results for volatile organics, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\060702\12735.D Vial: 11 Acq On 7 Jun 2002' 4:43 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 15 Phenol, 6-methyl-2-[(4-morp... Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 5.36 0.48 ug/L 333712 1,4-dichlorobenzene-d4 9.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenol, 6-methyl-2-[(4-morpholin... 207 C12H17NO2 060460-71-1 5 2 2-Ethylacridine 207 C15H13N 1000147-64-9 4 3 6,9,12,15,23,26,31, 34-Octaoxa-l,... 582 C24H46N4O8S2 110228-77-8 4 4 Borane, trifluoro- 68 BF3 007637-0772 2 Abundance Scan 389 (5.365 min): 12735.D (-385) (-) m/ z 49.10 10/6.00% 49 207 86 5000

5.00 5.20 5.40 5.60 5.80 ----- OA m/z 207.00 83.11% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #84739: Phenol, 6-methyl-2-[(4-morpholinyl)methyl]- 207 86

5000 121 500 5.20 5.40 5.60 5.80 57 m/z 86.00 66.44% 160

niz-> oL 50 444 —..00.1—0011 — । । i . . । 100 150 200250300350400450500550 । > i ■ i । । । । ■ ।

Abundance #84846:2-Ethylacridine 207 ' ■ I ' • ' 1 1 * 4 ‘ ' I ' ' ’ ' I ' 5.00 5.20 5.40 5.60 5.80 5000 m/z 208.00 41.32%

62 96 140166 O-r । । • 4/4, 14,4 r ■ ■ ‘ ■ i ■ ■ 1 1 i ■ ■ ■ ■ i 1 • ■ ■ i ‘ 1 ■ ■ i ■ ■ ■ ■ i 1 1 1 1 i 1 1 1 1 i miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #34760:6,9,12,15,23,26,31,34-Octaoxa-1,3,18,20-tetraazabi... 86 5.00 5.20 5.40 5.60 5.80 m/ 48.05 40.18%

5000 56 132 "Mhy"whaainonp 173

miz-> 0—" 50 u.n,.4—+ — A201231262.303— 348 433 468493521 100 150 200 250 300 350 400 450 500 550 582 11 ■ ■ ■ ■ i ■ ■ ■ ■ । ■ i ■ ■ ■ ■ । ■ ■ ■ ■ । 5.00 5.20 5.40 5.60 5.80

12735.D 060302.M Mon Jun 10 11:22:57 2002 Page 18

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