GCMS analysis results for sample AE10306, May 2002

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Data File C:\MSDCHEM\1\DATA\050802\10306.D Vial : 9 Acq On 8 May 2002 8:19 pm Operator: Mclean Sample 5/1 eh Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************** Peak Number 4 Hexanal Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 5.11 0.26 ug/L 263559 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexanal 100 C6H120 000066-25-1 22 2 Hexanal 100 C6H120 000066-25-114 3 Hexanal 100 C6H120 000066-25-1/14 4 Hexanal 100 C6H120 000066-25/1 12 Abundance Scan 346 (5.112 min): 10306.D (-341) (-) m/z 128.90 100.00% 44 56 129

5000 72 82 — 91 1 1 1 1 1 ' 1 1 I ' 1 1 1 1 1 1 ' 1 1 ‘ 1 1 1 I 50 4.80 5.00 5.20 5.40 Ol 11 ■ 1 ■ ■ i ■ ■ m/z 56.10 92.73% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #10785: Hexanal 44 56

5000 1 ' ' I ‘ 1 AMA.............. 1 1 । 1 ' 1 1 । . . . । . . . . । 29 4.80 5.00 5.20 5.40 72 82 m/ z 44.10 88.61%

m/z-> ol TTT 20 —38440 +50,4 30 50.1165114 50 60 70 80 | ' ■ I’l’t 90 । । 94 100 । 100 110 । 120 । , i । . । । . । 130 Abundance #110563: Hexanal 44 MMMNWA 56 4.80 5.00 5.20 5.40 27 5000 m/z 41.10 71.61%

72 82 01 TT——+ 1 , 37 15o. .... 11.... 4 rwhywWWporay ■i ' ■ 1 1 i 1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #110561: Hexanal ' l • ] 1 1 ■ ' I 1 I > < I ‘ 1 T1 1 111 « I 44 4.80 5.00 5.20 5.40 56 m/z 126.90 71.24%

5000 27

72 82

/z-> 0 TTP . 3& 1 + +24 50 I I I I 98 I I I I I I I ] I l I I I I I I I I I I I I

20 30 40 50 60 70 80 90 100 110 120 130 4.80 5.00 5.20 5.40

10306.D 050102.M Thu May 09 13:51:37 2002 Page 7

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