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GCMS analysis results for sample AE09333, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE09333 conducted on May 8, 2002.

NYC-WTC_000044628–000044649

Folder label: “GCMS X 4/29/02 A 5/3/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050202\9333.D Vial : 11 Acq On 2 May 2002 7:48 pm Operator: Mclean Sample 4/29 Inst : Instrumen Misc : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Hexanal Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

5.10 0.25 ug/L 191477 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexanal 100 C6H120 000066-25-1 2 Hexanal 100 C6H120 000066-25- 38 3 Hexanal 100 C6H120 000066-25 32 4 Hexanal 100 C6H120 000066- -1 32 Abundance Scan 343 (5.095 min): 9333.D (-339) (-) m/z 44.10 100.00% 44 56 129

5000 wwpoootWi oy* 72 82 I I-! ] ' I I I | I 1 । I | i > I > | । I ' ■

1 I I I I I I I I I I I I I 36 I I I | 1111111 13.......... 1.. Til I“| 11 i i । i i i | | i I T"1 | i i I I | i > I I | lill p 4.80 m/z 128.90 5.00 5.20 5.40 87.22% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #10785: Hexanal 44 56

5000 f I I I I I I I I I I > I I I I 1 I ] ' I > I-

29 4.80 5.00 5.20 5.40 72 m/ z 56.10 86.20% 82 1 1 ' r1 1 —L 50.1 1| ,1 1 65,1 ............... . 94 100 ' i 1 ■ r 1 I ■ ■ ■ ' i 1 ■ ■ ' I 1 ' 1 ' i 1 ' 1 1 i /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #110563: Hexanal 44 56 1 i ■ 1 1 1 i 1 1 1 ' 4.80 15.20 5.40 5.00 27 m/ z 41.10) 78.02% 5000

72 82 1 1 I ■ 1 ' 1 i ■ ' 1, 1 1 ' ' i 1 50 — ■ | | i i I I_ | i i I I |-1—r I I | r * I I | ' ' i ' m/z-> Abundance 10 20 30 40

44 50 60 70 80 #110562: Hexanal 90 100 110 120 130 "MAMh/N MAmh) hr ri । | 111" । t-i r_ f | i ) I । I l I । >

56 4.80 5.00 5.20 5.40 m/z 126.90 55.20% 5000 27 72 82 1 ■ i1 '''1 ।1' 15 1 Ipe i 11 38 I 50.1 |, 65 । | 1 I 1 1 ■ '1। । । i , , । । 100 । । । । । । । । । । । । । । । । । 1 ' i 1 1 ' 1 I 1 '' 1 । । । । । । । । n/z~> 10 20 30 40 50 60 70 80 90 100 110 120 130 4.80 5.00 5.20 5.40

9333.D 050102.M Mon May 06 13:55:56 2002 Page 9

NYC-WTC_000044637

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NYC-WTC_000044637Source: NYC Law Department, mirrored locally

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