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GCMS analysis results for unknown compounds, sample AE10201, May 2002

Machine-extracted title · confidence 95%

Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10201 on May 10, 2002.

NYC-WTC_000044959–000044977

Folder label: “GCMS X 4/30/02 A 5/8/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\10201.D Vial: 19 Acq On 9 May 2002 6:04 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 3 Hexanal Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.11 0.24 ug/L 260923 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexanal 100 C6H120 000066-25-1 38 2 Hexanal 100 C6H120 000066-25-1 35 3 Hexanal 100 C6H120 000066-25-1/35 4 Hexanal 100 C6H120 000066-25-1 32 Abundance Scan 345 (5.106 min): 10201 D (-340) (-) m/z 128.90 100.00% 129 44 56

5000 72 82 35 50 91 ' 1 1 1 1 ' ' 1 1 1 1 1 1 1 1 * ’ 1 TT 1 ' ' I

n/z-> Ol —IIl 4 |............. I... 10 20 30___ 40 50 60 70 1

80 I I

90 UI I I I I I I I

100 I I I I I

110 I I I I I

120 I I I I I

130 I I f I m/z 4.80 5.00 44.10 5.20 5.40 79.56% Abundance #110563: Hexanal 44 56

27 kwioow, ‘Wwwe 5000 ■ 1 ■ i ' ■ ■ ' i ■ ■ 1 1 i ' 1 1 ' i 1 1 1 ' I 4.80 5.00 5.20 5.40 72 82 m/z 56.10 76.91% 01 I I I I ■ I I I I I I. I I I I I I37 'I I I 50 LL 1 1 1 . .. I .... 1 ....1 .... 1 .... I > ! I I I TT+ ' I 1 ' ' 1 1 1 /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #110561: Hexanal 44 56 .................. ,.............. ) 1 1 1 1 1n 1 ' I ' z 1 1 1 1 1 1 1 I 1 1 1 1 I 4.80 5.00 5.20 5.40 5000 m/z 41.05 70.57% ’ 27

72 82

/z-> Abundance 01 .pnoiavs lpi ’ 10 20 30 38 50 +14 ‘I 1 1 ' ''I i'' 1 1 I|,1 1 1 ■ i > - ■98' I 1 1 1 1 I 1 1 1 1 I ' 1 ' 1 I ' 1 ' 1 I I 62 | | 40 50 60 70 80 90 100 110 120 130 44 56 #110562: Hexanal wwou 4.80 m/z 126.90 5.00 5.20 5.40 69.35%

5000 27 72 82

m/z-> 0 10 20 +— 15 38l 50.1 +654 .1 100 50 60 70 80 90 100 110 120 130 30 40 I "I I I 1 1 1 I ' 1 ’IJIIIII’II I 1 I I I I I I 1, ■ 1 i ' 1 ' 1 i 1 ' 1 1 i r ' 1 1 i 1 ■ ‘ ' i 4.80 5.00 5.20 5.40

10201.D 050102.M Thu May 09 13:37:07 2002 Page 7

NYC-WTC_000044970

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NYC-WTC_000044970Source: NYC Law Department, mirrored locally

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