GCMS analysis results for unknown compounds, sample AE10201, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\l\DATA\050802\10201.D Vial: 19 Acq On 9 May 2002 '6:04 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 2 Ethyl Chloride Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

3.76 0.37 ug/L 400479 1,4-Dichlorobenzene-d4 9.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethyl Chloride 64 C2H5C1 000075-00-3 4 2 2-Propanone, 1,1-dichloro- 126 C3H4C12O 000513-88-2 4 3 Acetic acid, dichloro-, ethyl ester 156 C4H6C12O2 000535-15-9/4 4 Acetic acid, dichloro-, ethyl ester 156 C4H6C12O2 000535-1579 4 Abundance Scan 116 (3.761 min): 10201 .D (-106) (-) m/z 43.10 100.00% 43 __

5000

■ ■ । > i ■ > ■ ■ । ■ ■ ■ > । ■ ' ■ ■ । ■ 59 83 3.40 360 3.80 4.00 4.20 35 -- - 01 ' i1 '1 ' i1 1 '' i ' *t m/z 83.00 9.87% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #107943: Ethyl Chloride 28

64 5000 340 3.60 3.80 4.00 4.20 49 m/z 50.. 10 6.85%

m/z-> 15 । .J I O+ .. IL 10 20 30 26

40 50 60 + 70 80 i11'•i1 1 1 1 i 90 100 110 120 130 140 150 160 Abundance #109152: 2-Propanone, 1,1-dichloro- 43 340 3.60 380 4.00 4.20 5000 m/z 84.90 6.16%

27 — Of mmmm 1 35 ’ 151 63..... 83 91..... 111 ,, 126.... m/z-> 10 20 30 •40 50 60 70 80 90 100 110 120 130 140 150 160 n/n M) 244 ,4 6. / Abundance #108006: Acetic acid, dichloro-, ethyl ester 29 3.40 3.60 3.80 4.00 4.20 m/z 4 9.10 5.53%

5000

15 48 83 0 -Hlrrr +37+444,, 57,65,73 , Il 93 101r 1 1 HI 1 i 123 140 154 i ■ 1 ' 1 i 1 ''' I 1 1 1 111 ■' ■ i 1 ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 3.40 3.60 3.80 4.00 4.20

10201 .D 050102.M Thu May 09 13:37:07 2002 Page 6

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