GCMS analysis results, sample AE09771, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C : \MSDCHEM\1\DATA\050602\9771 . D Vial: 24 Acq On 7 May 2002 6:25 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 9 Ethyl Chloride Concentration Rank. 10 R.T. EstConc Area Relative to ISTD R.T. 4.56 0.39 ug/L 232170 1,4-Dichlorobenzene-d4 9.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethyl Chloride 64 C2H5C1 000075-00-31 2 Propanoyl chloride 92 C3H5C1O 000079-03-81 3 2-Propenoyl chloride 90 C3H3C1O 000814-68-6 1 4 Nitrosyl chloride 65 CINO 002696-92-6 1 Abundance Scan 251 (4.554 min): 9771 .D (-249) (-) m/z 40.10 100.00% 4b WywMWNRMAw

5000 35 51 1 1 F' 1 83 88 4.20 4.40 4.60 4.80 5.00 । 1 1 I ' 1 1 ■ i 1 ■ 1 1 i 1 ■ 1 ' 1 1 1 I। I I । । । । I ' m/ z 35.10 27.59% 1 1 i ■ 1 1 ' । 1 1 1 ' । ' 1 1 । ■ m/z—> 0 10 20 30 40 50 60 70 80 90 100 Abundance #107943: Ethyl Chloride 28 M 64 5000 4 20 4.40 4.60 4.80 5.00 49 m/z 51.05 20.19% 15 35 1 ' i ■ ' 1 ' I 11 1 1 1 1 1 'I1'1 1 1 1 1I1 11 1 L1 ' 59.1 ' I1 ‘ i 1 ' 1 1 i ■ ■ ' ■ i 1 ■ ' ' i 1 m/z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #472: Propanoyl chloride 29 57 4 20 4.40 4.60 4.80 5.00 5000 m/z 49.10 17.22%

2 14 35 42 49 24 tr pa"boa 1’1 . ■ । 'i ,1 i 1 651 ■ ' 71i 1 1 76' ' i82' ' 1 1 911 1 1 1 1 1 1 "hruanpoimuapu. | , I I I | I'l1! 11 II n/z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #60: 2-Propenoyl chloride ■ ' I ' 1 27 55 4.20 4.40 4.60 4.80 5.00 m/z 83.00 14.26% ft 5000

35

n/z—> ............. 14 19 ,1 . , 11,40,45 50, +3.67.72 77 । 83 —90 T k

0 11 I I |

10 J il I [

20 I ki 10) ttlillJ t

30 40 t I I [t

50 60 70 80 90 100 ADAMAAMLMMLA/AJAAALAAALMA 4.20 4.40 4.60 4.80 5.00

9771.D 050102.M Tue May 07 15:44:21 2002 Page 12

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