GCMS analysis results for sample AE11420, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052002\11420.D Vial: 10 Acq On : 20 May 2002 8:37 pm Operator: Mclean Sample : 5/16 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Ethyl Chloride Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 3.75 0.30 ug/L 290057 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethyl Chloride 64 C2H5C1 000075-00-3 10 2 Pyrrolidine, 3-methyl- 85 C5H11N 034375-89-8 5 3 4-Penten-2-one 84 C5H80 013891-87-7 5 4 Ethanone, 1-oxiranyl- 86 C4H602 004401/11-0 5 Abundance Scan 114 (3.749 min): 11420.D (-103) (-) m/z 43.10 100.00% 43

5000

' I ' > > ' l « 35 86 3.40 3.60 3.80 4.00 Of ......... I'll.|h 17.. 58 i" 11 r 1" i H+ i111' i m/z 35.10 9.43% n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100

he Abundance #107943: Ethyl Chloride 23

64 5000 1 ' I ' 1 1 . 1 . 3.40 3.60 3.80 4.00 49 m/z 47.05 8.90% 35

m/z~> 01 ‘II‘ HH 15 I1'11111111 ■ -59++ i" " r1" i 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 p Abundance #7036: Pyrrolidine, 3-methyl- 43 WM/uMkasyoas 1 1 I . . ' ' I ' 3.40 3.60 3.80 4.00____ __ 5000 m/z 85.90 8.48%

28 85 "Mut—WMhyt MvWW 01 1 'i rn ■ 11 ■"15|"i1 20 51 56 61 68 75 80 ■ ।. 1/111,33/38 l I | I I II | I 1 t t| t 1'IT] I H I | I I I t | I I I I | I I I I [ I t I 91 " I"1' i " " i" m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #4029: 4-Penten-2-one 1 1 I 1 ' . ' I ' ' 1 ' 1 1 1 1 1 I 1 1 ' . I ' 43 3.40 3.60 3.80 4.00 m/z 50.10 8.10% 5000 WAAAA 15 27 38 50 55 69 84 0 THHH 111 ‘ " 11 ‘H111" i" " i1"11" " r 1 ‘11"'11"1 • i'." i" " i " 1 . I ’ ’ ' i 1 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 3.40 3.60 3.80 4.00

11420.D 050102.M Thu May 23 14:07:10 2002 Page 5

NYC-WTC_000025412