GCMS analysis results for sample AE11420, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052002\11420.D Vial: 10 Acq On : 20 May 2002 8:37 pm Operator: Mclean Sample : 5/16 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 1 Acetonitrile, dichloro- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 3.62 0.33 ug/L 313037 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0(86 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 45 3 3,3-Dichloropropyne 108 C3H2C12 1000222-23-9 23 4 Allyl mercaptan 74 C3H6S 000870-23-5 16 Abundance Scan 93 (3.626 min): 11420.D (-86) (-) m/z 74.00 100.00%! 7)4

82 5000 47 ............................... ............ .. 35

m/z-> Of -l—10 20 30 40 50 ' i • ' ' ' i ' 60 70 I T[33 80 1 ‘ i ' 90 ' i ' 1 ' 1 i ' 100 110 3.20 3.40 3.60 3.80 4.00 m/z 82.00 58.08%

Abundance #28338: Acetonitrile, dichloro- 74

5000 47 82 _A 3.20 3.40 3.60 3.80 4.00 m/z 84.00 55.01% 35

m/z—> 01

Abundance ..1012..... 20 26.30 Il40,.. .Ill,50 60 62 TIl ' ' I 1 ' ' ■ i ' 70 80 #115342: Acetonitrile, dichloro- , , 90 100 108 110 "M/ot 74 35 3.20 3.40 3.60 3.80 4.00 5000 82 m/ z 76.00 36.13%| 47

Of ' I ' Il ' ' In ■ ' ' TII 1 ' i ‘ 1 ' ' i 1 1 ' ' i ■ ' • ' i

A ■ ■ । ■ - - ■ । । 1 । ■ ■ ■ ■ । ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28312: 3,3-Dichloropropyne 74 3.20 3.40 3.60 3.80 4.00 m/z 47.10 27.38% 5000 38 47 0 28 11 '-I I ' 11111 ' 1 i 53 60 ,| 82 108 11 1 ‘IIt‘L1" m/z—> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.40 3.60 3.80 4.00

11420.D 050102.M Thu May 23 14:07:10 2002 Page 4

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