GCMS analysis results for sample AE06339, May 3 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050102\6339.D Vial : 15 Acq On 1 May 2002 9:06 pm Operator: Mclean Sample re-ext 4/29 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Acetonitrile, dichloro- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

3.65 0.37 ug/L 266116 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 90 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 72 3 3,3-Dichloropropyne 108 C3H2C12 1000222-23-9 25 4 Allyl mercaptan 74 C3H6S 000870-23-5 9 Abundance Scan 97 (3.649 min): 6339.D (-92) (-) m/ z 74.00 100.00% 74

82 5000

40 47 ..... M.S........ 3.40 3.60 3.80 4.00 ' 1 I ' ' 1 ' I 1 । । । ।' ।11' I- -p— ' i ' 1 1 1 i ' i TIB 1 1 i ■ 1 1 1 i 1 ' 1 ' i 1 m/z 82.00 53.52% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

5000 82 3.40 3.60 3.80 4.00 47 m/ Z 84.00 34.33% 35

m/z-> . 10....... 20 . 30 ll40 III50....6062....70 1 T9l 80 , 108 I ' । 1 1 ' 1 । 1 1 ■ ।■I 1 > 1 । I 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35 3.40 3.60 3.80 4.00 5000 82 m/z 76.00 32.30% 47

> > । ■ > > ■ । ’ ■ ■ ■ । • i-! | ‘ ' 'Tl 1 TBit 1 1 । ■ 1 ■ 1 । 1 ■ 1 1 । 1 1 1 ' i n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28312: 3,3-Dichloropropyne ■ ■ i i । I-! I i । i i i i । i i >< । l I-

74 3.40 3.60 3.80 4.00 m/z 47.00 25.68% ft 5000

/z-> 10 20 28 30 || 38

40 47 I i 53 60 ■ ■ i *‘‘1I‘*I 50 60 70 ,| 82 108 ■ i 1 1 ' 1 i r 1 ■ ■ i 1 1 1 ' i 1 1 1 1 i 80 90 100 110 M w"w I । | r I i i । I । । i | । i i r | i i

3.40 3.60 3.80 4.00

6339.D 050102.M Thu May 02 12:24:23 2002 Page 4

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