GCMS analysis results for sample AE10305, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\l\DATA\050802\10305R.D Vial: 26 Acq On 9 May 2002 12:56 pm Operator: Mclean Sample re-inj Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Acetonitrile, dichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 3.63 0.80 ug/L 652137 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0/90 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0-64 3 Allyl mercaptan 74 C3H6S 000870-23-5 5 4 3,3-Dichloropropyne 108 C3H2C12 1000222-23-9 4 Abundance Scan 93 (3.626 min): 10305R.D (-87) (-) m/z 74.00 10 0.00%| 74

82 5000

47 38 3.20 3.40 3.60 3.80 4.00 0+ ' ' 1 1 . ........ 1 1 ‘ 1/1 ' +r)l-, , ।. I ■ । । । ■ > ■ ■ । > ■ ■ ■ । m/z 82.00 50.75% n/z- > 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 7l4

5000 82 A 3.20 3.40 3.60 3.80 4.00 47 m/z 76.00 34.70% 35

mfe-> 01 12 > । T 1 1 1 1 I 1 '' >'' I 1 1 11 1 1 1 1 10 20 26 :30 -2—1 TIt | 108 1 • i ■ ' ‘ ■ i 1 1 1 1 1 1 1 ' 1 i 40 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35 3.20 3.40 3.60 3.80 4.00 5000 82 m/ z 84.00 33.37% 47

0 i । | > । i i । I 1 I [ r' r i I ■ 1 1'1 i *i ;11 ■ —TIB 11U———-——B—T—TTIRTTT n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28161: Allyl mercaptan 411 74 3.20 3.40 3.60 3.80 4.00 m/z 47.10 22.96% 5000 — 47 WWW wMM 0 T r [“I i I | | I 27 33 I [11153.57 I '| 1 I | ill 6841 ' 11 1 1 1 1 I ' 1 1 1 1 1 1 1 1 1 ' 1 I n/z-> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.40 3.60 3.80 4.00

10305R.D 050102.M Thu May 09 13:51:04 2002 Page 5

NYC-WTC_000045122