GCMS analysis results, sample AE09332, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\050902\9332 .D Vial: 22 Acq On : 10 May 2002 9:13 am Operator: Mclean Sample : 5/8 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 1 Acetonitrile, dichloro- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

3.61 0.29 ug/L 285417 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0(80 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 50 3 Allyl mercaptan 74 C3H6S 000870-23-5 25 4 Thiirane, methyl- 74 C3H6S 001072-43-1 5 Abundance Scan 90 (3.608 min): 9332.D (-84) (-) m/z 74.00 100.00% 74 82 5000

47 ................. ................................. 35 t 58 3.20 3.40 3.60 3.80 4.00 Of I f' ' । I । । । 1—H88, m/z 82.00 61.84% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

5000 82 । i । A 3.20 3.40 3.60 3.80 4.00 47 m/z 76.00 27.54% 35 0! .2— . . 62......... ! ■ ■ i 1 1 ■ ■ i ' "I4 ,1 ■ i ■ ■ ' ■ i ‘ 108 ' I ' ■ ■ ■ i

m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35 AA 3.20 3.40 3.60 3.80 4.00 5000- 82 m/z 47.10 23.56%

w.M rwMvw 47

01 1 ■ i ■ ' ‘ 1 i 1 ■ 1 ■ i ' • 1 _____________ L 1 ' i 1 ' ■ ■ i ■ ■ ■ ■ i ■ 1 ■ ‘ i 1 1 1 1 1 1 1 1 TBi miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28161: Allyl mercaptan 411 74 3.20 3.40 3.60 3.80 4.00 m/z 84.00 22.68%

5000 “Pw/sMot 47 0 .............. .. 1,535968,1 ' 1 I 1 1 1 । । ' । 1 1 । 1 1 1 । 1 ■ ■ ■ । ' ■ ■ ■ । r ■ ■ ■ । 1 ■ 1 ■ । m/z-> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.40 3.60 3.80 4.00

9332.D 050102.M Mon May 13 11:43:43 2002 Page 4

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