GCMS analysis results, sample AE09332, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\050902\9332.D Vial: 22 Acq On : 10 May 2002 9:13 am Operator: Mclean Sample : 5/8 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 2 Ethyl Chloride Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

3.73 0.39 ug/L 386379 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethyl Chloride 64 C2H5C1 000075-00-3 12 2 Acetic acid, dichloro-, ethyl ester 156 C4H6C12O2 000535-15-9 9 3 Acetic acid, dichloro-, ethyl ester 156 C4H6C12O2 000535-15-9 4 2-Chloroethanol 80 C2H5C1O 000107-07-3 /9 Abundance Scan 111 (3.731 min): 9332.D (-100) (-) m/ z 43.10 10 . 00% 43

5000 /W ■ ■ i ■ ■ ■ ■ i 1 ■ ■ 1 i ■ 1 ' ' । ■ 1 ' 1 । 86 35 O+ 11111'11 1111 It I, „7—?F-- m/z 3.40 3.60 49.10 3.80 4.00 13.54% m/z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160

23 #107943: Ethyl Chloride "MwWultty, 64 5000 3.40 3.60 3.80 4.00 49 m/z 86.00 13.33%

iz-> Abundance O+ - 15 I +4-H+HL 111 ’'' I''111''111'11' 111J * 111111'1111'1'' 111'' I' * 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 #334: Acetic acid, dichloro-, ethyl ester "MiraWPMMAuAwy, 23

3.40 3.60 3.80 4.00 5000 m/z 35.10 9.21%

48 83 19 |, 37, ,|„ 57 65 73 |1 93 102 111 121 129 141 155 Of 111—-dna‘0nmf—mftunmTO-T—T_TOTmOTOTU n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #108006: Acetic acid, dichloro-, ethyl ester 23 3.40 3.60 3.80 4.00 m/z 83.00 8.42%

5000

15 48 83

m/z-> 0 -— +87,44457 65,,73ml 93 101 111 123 140 154 ■ i ■' ■111'1 ■ i-''■1' ।'111111111111 * ।11111 > ■ 10 :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 A-Prn, , 1AAA, A n W ! i | , , Am 3.40 3.60 3.80 4.00

9332.D 050102.M Mon May 13 11:43:43 2002 Page 5

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