GCMS analysis results for sample AE10307, May 2002

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Data File C:\MSDCHEM\1\DATA\050802\10307.D Vial: 10 Acq On 8 May 2002 9:07 pm Operator: Mclean Sample 5/1 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Acetonitrile, dichloro- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 3.63 0.20 ug/L 197187 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 59 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 36 3 Allyl mercaptan 74 C3H6S 000870-23-5 32 4 Thiirane, methyl- 74 C3H6S 001072-43-1 5 Abundance Scan 94 (3.632 min): 10307.D (-89) (-) m/ z 74.00 100.00% 74

82 5000

38 47 NS.. 3.20 3.40 3.60 3.80 4.00 Of I I8,8 m/z 82.00 50.76% 111 ’ I’ 11/1001 miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

5000 82 3.20 3.40 3.60 1 3.80 4.00 47 m/z 84.00 48.91% 35 01 —2-2 62 , , 108 1 1 i ■ 1 ■ ■ i ' 1 • 1 1 1 1 ■ 11 1 1 ' ■ । ‘ TI3 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35 3.20 3.40 3.60 3.80 4.00 5000 82 m/z 76.00 27.38% 47 - +r 1 ‘id 1 1 i ‘ 1 1 1 1 1 1 ' 1 1 1 ' 1 1 I m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28161: Allyl mercaptan 41 74 3.20 3.40 3.60 3.80 4.00 m/z 47.00 24.90%

5000

27 33 । 47 59 co . JplopoJwAupi 0 —111170—+153 111 88 Tl /z-> 10 20 30 40। 50 60 70 80 90 100 110 3.20 3.40 3.60 3.80 4.00

10307.D 050102.M Thu May 09 13:52:06 2002 Page 4

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