GCMS analysis results for sample AE10816, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051302\10816.D Vial: 13 Acq On : 13 May 2002 9:16 pm Operator: Mclean Sample : 5/9 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Acetonitrile, dichloro- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

3.62 0.26 ug/L 235582 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 25 2 Allyl mercaptan 74 C3H6S 000870-23-516 3 Thiirane, methyl- 74 C3H6S 001072-43-1 9 4 Ethyl ether 74 C4H10O 000060-29-7 4 Abundance Scan 92 (3.620 min): 10816.D (-86) (-) m/z 74.00 100.00% 74

82 5000 47 —

m/z-> 01 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i11 ■1 i ■ ■ 15 20 25 30 35 40 45 50 55 60 mm _ei 58 joBapos 65 I 11t 11i’ 70 75 80 35 i11 ■' i1'1' i 85 90 95 3.20 m/z 3.40 82.00 3.60 3.80 4.00 51.29% Abundance #115342: Acetonitrile, dichloro- 74 35

5000 82 .. ..he...... 3.20 3.40 3.60 3.80 4.00 88 47 m/z 84.00 43.50%

m/z—> 0! ■i■ ■ ■' । ■" ■ । ■■■■ i ■' +0 86 rh.. ।. I. TT 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #28161: Allyl mercaptan 41 74 i ■ ■ ■ ■ i ' ' 3.20 3.40 3.60 3.80 4.00 5000 m/ z 76.00 42.23% 45

- 3&

miz-> 0! . ............. 15 20 25 30 35 40 148 53 5659 111111111 j j 11111 j 1111

45 50 55 60 —65 6871 1111 ■ i ■'111'1111 ■ ■ ■' i

70 75 80 85 90 95 Abundance #115343: Thiirane, methyl- I ' ' ' 1 I ' ' 41 74 3.20 3.40 3.60 3.80 4.00 m/z 47.05 27.64%

5000 45 AAAL.... , 27 — 23 38 /z-> 24 . । 30 00 0 ■ i ■ ■ ■11' nrrtti ?11111 ] 1111 15 20 25 30 35 t

40 148 53 56 I 11111111 ~i~ 111 45 50 55 5164.6871. 60 65 70 75 80 85 90 95 3.20 3.40 3.60 3.80 4.00

10816.D 050102 .M Tue May 14 11:42:54 2002 Page 4

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