GCMS analysis results, sample AE09971, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050602\9977.D Vial : 19 Acq On 7 May 2002 2:22 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Acetonitrile, dichloro- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

3.61 0.42 ug/L 279590 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12 -090 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0(83 3 3,3-Dichloropropyne 108 C3H2C12 1000222-23-9 33 4 Allyl mercaptan 74 C3H6S 000870-23-5 7 Abundance Scan 90 (3.608 min): 9977.D (-85) (-) m/z 74.00 100.00% 74

5000 82

47 _ । । । । । । । । । । । ______________________■ । । । । । । । । । । । 35 3.20 3.40 3.60 3.80 4.00 .................... 1,141 , 1 1 I Illi I I I kl J I I I I I . . ................ 1 , i8,8 m-1 1 i i [ । । । । । । । । । । । > ' i T m/z 82.00 46.04% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

5000 47 82 3.20 3.40 3.60 w ■ ■ । 3.80 ■ I । ■ 4.00 m/z 84.00 32.25% 35

/z-> 12 । ' I ’ ' ' । I । 1,1 1 ' 10 20 26. , 62......... । 30 1 1 I 1 1 I I I I I I 40 50 60 pi11!1 70 80 "bit ,I • i ■ ■ ■ ■ । 90 100 108 ■ 1 I ■ ■ ■ ■ ।

110 MW_Wpt Abundance #115342: Acetonitrile, dichloro- 74 35 3.20 3.40 3.60 3.80 4.00 5000 82 m/z 76.00 30.37% 47

i > | i i > I | I I I r [ I I lir rthi- r , 1 i 1 1 1 1 1 1 TIl 11 I t I I 1 ] * l 1 1 1 I-1 1 [

m/z--> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28312: 3,3-Dichloropropyne .......... 34.... | I । I I | I i i । । । i ri । i i

74 3.20 4.00 3.40 3.60 3.80 m/ z 47.05 19.35% __ 5000 38 47

■ ‘ । ■ 1 1 1 । ■ i I I । । i’। 28 II L। i r I l 53 60 TTI’’r ' 'J 1 r 1 ' I1 ,| 82 .............. 108 I 1 ■ ' ■ I 1 1 1 1 I ■ 1 ■ 1 I 1 ' I > I > > Tl/Z"> 10 20 30 40 50 60 70 80 ' 90 100 110 3.20 3.40 3.60 3.80 4.00

9977 ,D 050102.M Tue May 07 15:54:22 2002 Page 6

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