GCMS analysis results, sample AE09971, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050602\9977.D Vial: 19 Acq On 7 May 2002 2:22 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Methane, bromodichloro- Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 3.33 0.33 ug/L 220467 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methane, bromodichloro- 162 CHBrC12 000075-27-4 83 2 Chloroform 118 CHC13 000067-66-3 72 3 Chloroform 118 CHC13 000067-66-3 72 4 Methane, bromodichloro- 162 CHBrC12 000075-27-4 59 Abundance Scan 42 (3.326 min): 9977.D (-34) (-) m/z 83.00 100.00% 83

5000

47 .....p.... „ ‘ ' । | ' I ' I | । I । । | । I । । | r r i I | I I I t | TI I 1 | t 129 3.20 3.30 3.40 3.50 3.60 3.70

m/z-> ''' i' 1111'11' l ‘ 10 20 30 35 +.58. 67, 40 50 60 70 il T 80 i ■ ■ > ■ । 11 , ■111' 90 100 110 120 130 140 150 160 170 i11' ■ i m/ z 85.00 62.34% Abundance #116506: Methane, bromodichloro- 83

A A A / V A M I 5000 ’’’11/1 1 l ) I ! > > ] l i. I | . . < I | I I T ! | III r | I

3.20 3.30 3 40 3.50 3.60 3.70 47 129 m/z 47.10 15.38% 35 III, 55 64 72 m/z—> 1 1 I 10 13 1 1 I 11 '1 I '''1 20 30 I I I I rI I 1 I I I I I > I I I I >

40 50 60 70 —80+ 19190 100 110116120 130 140144150 160163170 || i । । । । । । । t r r ।' । r i r | r I 11111 '111 r'11 11

Abundance #116498: Chloroform 83 1' i 11 1 11 11' ■ i'11 ■ srrrumrU" |i > ■ 111 3.20 3.30 3.40 3.50 3.60 3.70 5000 m/z 128.90 12 .80% 47 35 13 | 118 ■ ■i > i ■, H prill, ,,, 1 70 r ' ■ ■ i11' ■ 11’1 । 1 1111411/111 TTT11 | , , | | | , rii| i I m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #116499: Chloroform 11’1 1 111 11 11 83 3.20 3.30 3.40 3.50 3.60 3.70 m/z 86.90 10 .23% ft 5000

47

m/z-> 35 h । < । ' । । । । । । ' । । । I 111 | ri "i li1f' I I I i | i

10 20 30 40 50 60 70 TII 70 TH — 80 118 —euu—;uIDTT TTTT 90 100 110 120 130 140 150 160 170 ,, I... fl...... 3.20 3.30 3.40 3.50 3.60 3.70

9977.D 050102.M Tue May 07 15:54:22 2002 Page 5

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