GCMS analysis results for sample AE11421, May 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052002\11421.D Vial: 11 Acq On : 20 May 2002 9:26 pm Operator: Mclean Sample : 5/16 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 1 Methane, bromodichioro- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

3.32 0.37 ug/L 289280 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Methane, bromodichloro- 162 CHBrC12 000075-27-4 2 Methane, bromodichloro- 162 CHBrC12 000075-27-4 y 3 3 Chloroform 118 CHC13 000067-66-3/78 4 Methane, bromodichloro-_____________ 162 CHBrC12 000075-27- A 74 Abundance Scan 41 (3.320 min): 11421 .D (-34) (-) m/z 83.00 100 . 00% 83

5000

47 20* mnf 129 3.20 3.30 3.40 3.50 3.60 3.70

m/z—> 0 37 | 58 , I I I , , , ! , , , , I , ,',1, | | I rile, I H ! I ! I I | | I , 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 . + ll,' gI' । । । । । । । । j । । । । । । । । > । । । rm | I I 1 1 ! I ! I I | I I ! I | , I r1 e m/ z 85.00 56.05% Abundance #33236: Methane, bromodichloro- 83

5000 _/W 11 ‘I > fi । । i i i । । । । । । । > > i >■[ > rr. 11 n "I 3.20 3.30 3.40 3.50 3.60 3.70 47 m/z 47.05 15.93% 129 93 0- . ........... . 164 TT ■।■111■1111■■111'*1'।1'''।'11''1 ■ ।1 • 116 ||, miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #116497: Methane, bromodichloro- 83 “ [ " 111 " 1 'lTn > I “ 1 ‘ I'11111 " 11 3,20 3.30 3.40 3.50 3.60 3.70 5000 m/z 128.90 11.48%

47

01 .... 38,27), 60............. 191 .................. II............................. II 1+ ' 11''' 11'1 ’ 11' 129 11''1' i'''' r ' ■' i'111111111r 11 ■ ।1111111 m/z-> 10 20 30 70 80 90 100 110 120 130 140 150 160 170 40 50 Abundance #116498: Chloroform 11 " 111'1111''1' I 83 3,20 3.30 3.40 3.50 3.60 3.70

wu m/z 48.10 10.62% ( 5000

35 47 Mwwl 13 I" 11 'I1'1 sslana 70 | 118 0 TITHT 11" " I " " I " ■111'1' i ■" 111' rli ■" ■ i1 ■ ■ ■ । ■11 ■ i' ■1 ■ i11' ■ । ■1 I’I’’’IE’’AAI’’’’A’’A’I’+’’II’I’I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 3.20 3.30 3.40 3.50 3.60 3.70

11421.D 050102.M Thu May 23 10:48:23 2002 Page 4

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