GCMS analysis results for unknown compounds, sample AE10202, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\10202.D Vial: 20 Acq On 9 May 2002 6:53 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 1 Methane, bromodichloro- Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

3.37 0.23 ug/L 271051 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methane, bromodichloro- 162 CHBrC12 000075-27-4 83 2 Chloroform 118 CHC13 000067-66-3 80 3 Methane, bromodichloro- 162 CHBrC12 000075-27-4 78 4 Methane, oxybis[dichloro- 182 C2H2C140 020524-86-1 56 Abundance Scan 49 (3.367 min): 10202.D (-42) (-) m/z 83.00 100.00% 83

5000

47 fo 14 auum/Mi 129 3.20 3.30 3.40 3.50 3.60 3.70 3.80 35 ol 1 ■ r 1 ■11 ■11111 ’ 11 1.58 It II, m/ z 85.00 69.81% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #116506: Methane, bromodichloro- 83 ■

5000 r ‘"t !iii । i i i rp rtT| r r । । | > ill I । f । i J । 1 3.20 3.30 3.40 3.50 3.60 3.70 3.80 47 129 m/z 47.00 22.10% 13 35 , Ik 55 64 72 H |9,! 116 11 144 163 0) TTIPTTITTTTTTT 711 I* I I I I I I I I I I I I I I I I I l I I I 1 1 I I I I I ] I 1 I • I 1 1 I I I > I I I I I I I I [ I 1 I I I I'l l

m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #116499: Chloroform 83

3.20 3.30 3.40 3.50 3.60 3.70 3.80 5000 m/ z 48.05 14.08%

35 । 47 w. m/z-> 70 0 TTITTITTTTTTTTTTTTT ■ । ■ ■ ■ ■ । ■ | —Pppt 118 T i'111 r ■ ■1111 ■ ■ r 1111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Ww Abundance #33236: Methane, bromodichloro- 1111111 r 1111'111 r 1111111' i ’1■■i'1 83 3.20 3.30 3.40 3.50 3.60 3.70 3.80 m/ z 87.00 13.94%

5000

47 129 13..... 27 35..... !||,..... 63 72 j,, | 93 116 ||, 164 0 11■1■11■1111■■1■i11111'■■■i11 ■ ■ i1'1 'i1 r 11111'1 j 1111 r ‘1' i m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 3.203.30 3.40 3.50 3.60 3.70 3.80

10202.D 050102.M Thu May 09 13:37:30 2002 Page 5

NYC-WTC_000045029