GCMS analysis results, sample AE09154, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\050902\9154.D Vial: 19 Acq On : 10 May 2002 6:47 am Operator: Mclean Sample : 5/8 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 1 Methane, bromodichloro- Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

3.29 0.25 ug/L 201048 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methane, bromodichloro- 162 CHBrC12 000075-27-4 83 2 Chloroform 118 CHC13 000067-66-3 78 3 Methane, oxybis[dichloro- 182 C2H2C140 020524-86-1 78 4 Methane, bromodichloro- 162 CHBrC12 000075-27-4 74 Abundance Scan 36 (3.290 min): 9154.D (-31) (-) m/z 83.00 100.00% 83

5000

44114 ..... . ...... .. 35 47 129 3.20 3.30 3.40 3.50 3.60 3.70 _58 ol 111"1'i1" 111" 1111 ■11 ।111 ........... I III ........... r.............. m/ Z 85.00 73.21% nz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #33236: Methane, bromodichloro- 83

5000 Ar AiiA MH r 3.20 3.30 3.40 3.50 3.60 3.70 47 m/z 47.10 :17.82% 129 ,,13.....27 35..... |||...... 63 712 । [ 93 116 || 164 Of 1111111111111111111 ■111 ■'111' ■'' i' ■' ii

LM. W T*Cumn"m——OODTT i1 ■" i11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #33238: Chloroform 83 3.20 3.30 3.40 3.50 3.60 3.70 5000 m/ z 35.10 11.58% 47 35 27 O+ 1*1’1111000117 -6070.71XTTTOIIm* 96 118 WMN miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #33237: Methane, oxybis[dichloro- ' I ‘ ‘ 83 3.20 3.30 3.40 3.50 3.60 3.70 m/z 87.00 11.37%

5000 47 28

n/z-> 0 TII’ +47 I — 70 III 111" 111111 IT 111.. 11... 1, 11111,1111111111111'... I... 111. 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 ’ I’’ ............ i' ‘111' ■' ■ i' ■' ‘ i ■ ■ ■ ■ i'' 3.20 3.30 3.40 3.50 3.60 3.70

9154.D 050102.M Mon May 13 11:28:45 2002 Page 4

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