GCMS analysis results, sample AE09154, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\050902\9154.D Vial: 19 Acq On : 10 May 2002 6:47 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L *************************** * * **************************************** Peak Number 2 Chloromethyl ethanoate Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

3.72 0.28 ug/L 229643 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Chloromethyl ethanoate 108 C3H5C1O2 1000143-34-6 4 2 Ethyl Chloride 64 C2H5C1 000075-00-3 • 3 Ethanol, 2,2-dichloro- 114 C2H4C120 000598-38-9 2 4 Acetic acid, chloro-, ethyl ester 122 C4H7C1O2 000105-39-5 1 Abundance Scan 109 (3.719 min): 9154.D (-100) (-) m/ z 43.10 100.00% A 43

nuto/yuakar/WAANA. 5000 49

35 59 86

+ ' ' ' I 1 ' ' ‘ I ' ' ' 1 I ' ' ' ‘ I ‘ ' I 3.40 3,60 3.80 4.00 Of 1 ' i ' ' ■ ' i ' ' ' 1 i ' - ■ l ■ ‘ 1 1 1 1 ............................ -.... — ........ - m/z 49.10 40.24% niz- > 10 20 30 40 50 60 70 80 90 100 110 120 Abundance 43 #4957: Chloromethyl ethanoate "uAnyhowiup 5000 ■ । > । i । । । । ■ ■ ■ ■ । ■ ■ ■ ■ । 3.40 3.60 3.80 4.00 49 m/z 86.00 21.91% 73

miz- > 01 - 10 20 30 40 ' ■ i ' ■ ' ‘ i 1 ' ■ ■ i ■ ' ■ ' i ' ■ ‘ ■ i ' 1 • ' i ■ ' ' ■ i ' ' ' 1 i ‘ ■ 50 60 70 80 90 100 110 120 "MMh-wy/uMMWh4 Abundance #107943: Ethyl Chloride 23

3.40 3.60 3.80 4.00 64 m/z 35.10 17.71% 5000

49 35 0! —IP 15 I'1 1, i' ■ i ■ • ' 1 I ■ 1 ‘ 1 1 ‘ ■ 1 1 ' ' ■ i ' 1 ■ ■ i ■ ■ A p m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #1082: Ethanol, 2,2-dichloro- 31 3.40 3.60 3.80 4.00 m/ z 59.10 17.13%

5000

Tl/Z-> 0 -2+4 10 20 30 37 43 49 55 61 70 77, 83 1————aumH]mTETDTT 40 50 60 70 80 96 103 114 90 100 110 120 3.40 3.60 3.80 4.00

9154.D 050102.M Mon May 13 11:28:46 2002 Page 5

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