GCMS analysis results, sample AE09154, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\050902\9154.D Vial: 19 Acq On : 10 May 2002 6:47 am Operator: Mclean Sample : 5/8 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 2H-Pyran, tetrahydro- Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

5.08 0.24 ug/L 196243 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2H-Pyran, tetrahydro- 86 C5H10O 000142-68-7 8 2 2H-Pyran, tetrahydro- 86 C5H10O 000142-68-7 9 3 2H-Pyran, tetrahydro- 86 C5H10O 000142-68-7 9 4 Piperidine, 3-isopropyl- 127 C8H17N 1000197/57-3 9 Abundance Scan 340 (5.077 min): 9154.D (-335) (-) m/ z 44.10 100.00% 4l4

5000 56 84 129 thbwlpptt WWu 72 —■ 1 1 ■ i ' 1 ■ 1 i 1 ■ ■ 1 i ■ 1 1 1 i ■ ' ■ ' 4.80 5.00 5.20 5.40

miz-> 0- ■ ■ i ■ ' 1 ■ i ■ ' ■ ■ i ■ ' 10 20 30 1 4- 40 50 60 1 i ■ ■ ■ ■ i 70 80 1 ■ ' I 90 100 ' 1111111'1111 ■1 ■ ■ । ■ ■ ■ ■ । 110 120 130 ‘ । m/z 41.10 67.95%

Abundance #108883: 2H-Pyran, tetrahydro- 41

5000 28 56 85 Mtuhee” m/z 4.80 5.00 56.10 5.20 5.40 42.79%

miz-> o1 15 jeas 441144594 10 20 I 30 40 50 60 L 70 80 90 100 ' i ■ ■ ■ ■ i ■ ■ 1 ■ i ■ ■ ' ■ i ■ ■ ■ ■ i ■ ■ ' ' i 110 120 130 Abundance #108678: 2H-Pyran, tetrahydro- 41 . .................. ill , , 56 4.80 5.00 5.20 5.40 28 85 5000 m/z 128.80 41.51%

0- -PP—44 +524 1.67,73. 1 1 ' 1 1 1 I' • ' 1 I ‘ - । ■ ■ ■ ■ i > । ‘ ■ i ■ ■ ■ > i ■ ■ ■ ■ i ■ ■ ■ ■ i n/z-> 10 50 20 60 70 30 80 90 100 110 120 130 40 Abundance #108679: 2H-Pyran, tetrahydro- 41 4.80 5.00 5.20 5.40 m/z 57.10 36.06% 56 28 85 5000

0 * +594 MU 1801 ll,90/ 00100007 Tl/Z-> 10 20 30 40 50 60 100 110 120 130 70 4.80 5.00 5.20 5.40

9154.D 050102.M Mon May 13 11:28:47 2002 Page 6

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