GCMS analysis results for sample AE11932, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report • ‘ Data File : C:\MSDCHEM\l\DATA\052302\11932.D Vial: 12 Acq On : 23 May 2002 6:56 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 Pyridine-d5- Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T.

4.48 0.49 ug/L 338402 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qu.

1 Pyridine-d5- 84 C5D5N 007291-22-7/7 2 Perdeuterobenzene 84 C6D6 001076-43-3 5 3 Ethyl Chloride 64 C2H5C1 000075-00-3 2 4 Boron trifluoride etherate 142 C4H10BF3O 000109-63-7 2 Abundance Scan 238 (4.478 min): 11932.D (-236) (-) m/z 49.10 00.00% 48 84

5000 35 44 52 41 70 58 4.20 4.40 4.60 4.80 O+ ■ ■ i “ ■ ■ i ■■ ■ ■ i ‘' ■ i “ i ■ ■ “ i “ -qTrrrp-rrTp-rTT "' i1"11' 11" i •" ■ i m/z 84.00 88.47% niz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #33686: Pyridine-d5- 56 84

5000 52 1 ' I ' ' ' • i ■ ‘ ‘ i ' ■ ■ ■ i ■ ■ 28 4.20 4.40 4.60 4.80 38 42 m/z 35.10 40.13%

niz-> Abundance 14 O+ 1‘11111111'1111'' 11 341.132,1.1 5 24 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 #33650: Perdeuterobenzene TTTN 48 + 62 66 76 ' I' ■1 ■ i111111"' i ■ MMMk Ar 84

4.20 4.40 4.60 4.80 5000 m/z 44.00 33.49%

niz-> Ot 5 .................................................... 42

10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 48 52 56

62 6672 76 80 Immm _Tm M Abundance #107943: Ethyl Chloride 1+ T 177 23 4.20 4.40 4.60 4.80 m/z 52.10 30.49% 64 5000

49 25 31.2s, 1215 TTTT ,, , 60 67 5 nilAians 0- ■ ।>»1111 ■ i■ ■.■ i1 'll I?..।. • i ■ “11 ■ •" i “ “ I “ ■ ■ i 1 ' i 1 • ‘ । / 1 i 1 ■ • i ■ ■ miz—> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.20 4.40 4.60 4.80

11932.D 052202.M Wed May 29 09:51:37 2002 Page 13

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