GCMS analysis report, sample AE12763, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\060602\12763.D Vial: 9 Acq On 6 Jun 2002 5:49 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 Pyridine-d5- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 3.97 3.78 ug/L 3228650 1,4-dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyridine-d5- 84 C5D5N 007291-22-7/9 2 Methylene Chloride 84 CH2C12 000075-09-/ 9 3 Thiophene 84 C4H4S 000110-02/1 7 4 Thiophene 84 C4H4S 000110-02-1 5 Abundance Scan 152 (3.972 min): 12763.D (-150) (-) m/z . 84.00 00.00% 84

49 5000

35 41 52 88 3.60 3.80 4.00 4.20 4.40 38 44 Ol " i" " i ■" ■ i ■" ■ i" " i" " i" " "1 ■ i THut m TTTTTT m/z .49.10 60.00% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33686: Pyridine-d5- 50 84

5000 52 28 3 60 3.80 4.00 4.20 4.40 38 42 m/z 35.10 20.97% /...

mtz—> 5 14 24, ol " i"'' i ■1" i '■' ■ i" " i11 1 32.44.++484+ 10 15 2025303540 45 50556065 70 75 80859095 , l■■1" 62 66 76 ।i ■ ■ ■■ i1 ■111■l■ | ■ i “' ■ i"

Abundance #111040: Methylene Chloride 40 84 3.60 3.80 4.00 4.20 4.40 5000 rn/z 41.10 18.19%

miz-> 14 2528 32 ol —HTPT 111 " । ■ |1"' । Fi 11111111 5 35 0841 70 +2 1111>11< 1 ■ ■ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ■ i ■ ■ ■ ■ i ■ ■ ‘ ■ i' ■ ■ ■ 11 ■" i ■ ■ “ i"1 88 WMmapn, Abundance #116584: Thiophene 1 t 1 ■ ■ ■ i ■ ' ■ ■ i ■ 1 1 1 i ' 1 84 360 3.80 4.00 4.20 4.40 58 m/z 81.90 13.13% 45 5000 39 50 0 .... ........ 42 i ii11111111 ++++ 6972 HmmH 81 87 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20 4.40

12763.D 060302 .M Mon Jun 10 10:29:05 2002 Page 12

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