GCMS sample analysis results, AE11902, June 3, 2002

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Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11902.

NYC-WTC_000012881–000012907

Folder label: “GCMS X 5-21-02 A 5-22-02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052202\11902.D Vial: 9 Acq On : 22 May 2002 8:20 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 2-Ethylacridine Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 5.38 0.64 ug/L 414781 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Ethylacridine 207 C15H13N 1000147-64-9 9 2 3,5-Dimethylbenzaldehyde thiocar... 207 C10H13N3S 1000195-15-1 9 3 2-(1-Piperidino)-5-nitropyridine 207 C10H13N3O2 026820-61-1 9 4 Cyclotrisiloxane, hexamethyl- 222 C6H1803Si3 000541-05-9 9 Abundance Scan 391 (5.376 min): 11902.D (-380) (-) m/z 207.00 00.00% 207

t 5000 84 48 96

miz-> 0 ‘ ■ i • ■ “ i ■1 “ i • Tgu . . 2. . . 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 191 5 00 ^m/z^^^ 5.20 5.40 5.60 5.80

Abundance #84846:2-Ethylacridine 192 27

5000 500 ' 5.20 5.40 5.60 5.80 m/z 48.00 25.40%

miz-> 01 -777pptp.$2.,,76,—48£+114124,140.151.,166,178.llpl,— "MMMaptM,, 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #84771:3,5-Dimethylbenzaldehyde thiocarbamoylhydrazone 132 207 76 ' i ■ ■ ■ ■ i ■ ■ ■ 1 i ■ ■ ■ ' i • ' ‘ ' i ■ 43 500 5.20 5.40 5.60 5.80 5000 m/z 96.10 23.96! 60 147 27 163 174 190 , 0 44 fri l 7# l, ■ n # mpmpmmm TTTTT miz-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #84816:2-(1-Piperidino)-5-nitropyridine ' I ' ' ' ‘ I ' ‘ ' I ‘ ‘ ‘ I ' ' 207 5.00 5.20 5.40 5.60 5.80 178 m/z 209.00 21.15 124 5000 84 164 152 42 56 139 192 69 106 93 O Tp-TTTp-rJu+lueppalkpeApdl..,7R.., — mp U 1 I ' ' 1 ' 1 1 1 n/z—> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 5.00 5.20 5.40 5.60 5.80

11902.D 052202.M Tue May 28 12:06:48 2002 Page 17

NYC-WTC_000012902

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GCMS sample analysis results, AE11907, June 4, 2002 · Box DEP Box 15

NYC-WTC_000012989

Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.

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