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GCMS calibration data for sample AE11931, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11931 conducted on May 29, 2002.

NYC-WTC_000013574–000013602

Folder label: “GCMS X 5/22/02 A 5/23/02

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Scanned page image, NYC-WTC_000013591
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052302\11931.D Vial: 11 Acq On : 23 May 2002 6:07 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 11 3,5-Dimethylbenzaldehyde th... Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

5.36 0.45 ug/L 274748 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,5-Dimethylbenzaldehyde thiocar... 207 C10H13N3S 1000195-15-1 9 2 N-Methyl-l-adamantaneacetamide 207 C13H21NO 1000211-60-49 3 Cyclotrisiloxane, hexamethyl- 222 C6H1803S13 000541-05-2 9 4 Cyclotrisiloxane, hexamethyl - 222 C6H1803Si3 000541-05-9 9 Abundance Scan 389 (5.365 min): 11931 .D (-385) (-) m/z 207.00 100.00% 2(7

5000 49 86 58 96 133 191 38 5.00 5.20 5.40 5.60 5.80 01 ’I’E’’ITT L I''' ‘ I ‘ ‘ ' I ' 1’3 ■i■■1■i “ ‘'i'*■■i “ i■1■■i “'■i■■ “ i “ ‘■i11 “ i “ ■ ■ i •' ‘ ■p-rTT m/z 86.00 37.27% niz—> 2030405060 70 8090 100110120130140150160170180190200210 * Abundance #84771:3,5-DimethylbenzaIdehyde thiocarbamoylhydrazone 132 2(17 "Was 76 43 5000 60 '560' 5.20 5.40 5.60 5.80 91 105. 147 m/z 49.10 36.53% . 116 27 163 174 190 0- - +4444 TT trirroef Ayr -TTp niz-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #84775: N-Methyl-1 -adamantaneacetamide 207 135 500 5.20 5.40 5.60 5.80 5000 73 58 93 41

niz-> + 4 H+| 107 119 | 0! ‘ I ‘ ‘ “ I ' ' mterr +-p-rm mmpm 20- 30 40 50 60 70 80 90 100110120130140150160170180190200210 ■JTTTT 150 164 176 192

Abundance #126481: Cyclotrisiloxane, hexamethyl- ' ‘ I ' ' ‘ ‘ I ' ‘ 1 ' I ' ' ' ' I ' 1 1 ' 1 1 207 500 5.20 5.40 5.60 5.80 m/z 96.20 24.84% 5000

133, 191 119 147 163 177 L 0 .|>II ..... | I ... | I ........[r | I <! 1 | 1 1 11 | 1'1 I I ‘1’ 4 Tppgga Tuu ‘ ‘ I ' • ‘ ‘ ’ -r-r-p-r-r-r-j-T m/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 5.00 5.20 5.40 5.60 5.80

11931.D 052202.M Wed May 29 09:51:00 2002 Page 14

NYC-WTC_000013591

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NYC-WTC_000013591Source: NYC Law Department, mirrored locally

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