NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\052302\11931.D Vial: 11
Acq On : 23 May 2002 6:07 pm Operator: Mclean
Sample : 5/22ad Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
*********************************************************************
Peak Number 11 3,5-Dimethylbenzaldehyde th... Concentration Rank 17
R.T. EstConc Area Relative to ISTD R.T.
5.36 0.45 ug/L 274748 1,4-Dichlorobenzene-d4 9.90
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3,5-Dimethylbenzaldehyde thiocar... 207 C10H13N3S 1000195-15-1 9
2 N-Methyl-l-adamantaneacetamide 207 C13H21NO 1000211-60-49
3 Cyclotrisiloxane, hexamethyl- 222 C6H1803S13 000541-05-2 9
4 Cyclotrisiloxane, hexamethyl - 222 C6H1803Si3 000541-05-9 9
Abundance Scan 389 (5.365 min): 11931 .D (-385) (-) m/z 207.00 100.00%
2(7
5000
49 86
58 96 133 191
38
5.00 5.20 5.40 5.60 5.80
01 ’I’E’’ITT L
I''' ‘ I ‘ ‘ ' I ' 1’3 ■i■■1■i “ ‘'i'*■■i “ i■1■■i “'■i■■ “ i “ ‘■i11 “ i “ ■ ■ i •' ‘ ■p-rTT
m/z 86.00 37.27%
niz—> 2030405060 70 8090 100110120130140150160170180190200210 *
Abundance #84771:3,5-DimethylbenzaIdehyde thiocarbamoylhydrazone
132 2(17 "Was
76
43
5000
60 '560' 5.20 5.40 5.60 5.80
91 105. 147 m/z 49.10 36.53%
. 116
27 163 174 190
0- - +4444 TT trirroef Ayr -TTp
niz-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210
Abundance #84775: N-Methyl-1 -adamantaneacetamide
207
135
500 5.20 5.40 5.60 5.80
5000
73
58 93
41
niz->
+ 4 H+| 107 119 |
0! ‘ I ‘ ‘ “ I ' ' mterr +-p-rm mmpm
20- 30 40 50 60 70 80 90 100110120130140150160170180190200210
■JTTTT
150 164 176 192
Abundance #126481: Cyclotrisiloxane, hexamethyl- ' ‘ I ' ' ‘ ‘ I ' ‘ 1 ' I ' ' ' ' I ' 1 1 ' 1 1
207 500 5.20 5.40 5.60 5.80
m/z 96.20 24.84%
5000
133, 191
119 147 163 177 L
0 .|>II .....
| I ... | I ........[r | I <! 1 | 1 1 11 | 1'1
I I ‘1’ 4 Tppgga Tuu ‘ ‘ I ' • ‘ ‘ ’ -r-r-p-r-r-r-j-T
m/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 5.00 5.20 5.40 5.60 5.80
11931.D 052202.M Wed May 29 09:51:00 2002 Page 14
NYC-WTC_000013591
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