GCMS analysis results for sample AE11929, June 2002

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Laboratory report documenting GCMS analysis of sample AE11929 conducted on June 4, 2002.

NYC-WTC_000013524–000013550

Folder label: “GCMS X 5/22/02 A 5/23/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\11929.D Vial: 9 Acq On : 23 May 2002 4:29 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 2-Ethylacridine Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

5.37 0.33 ug/L 236894 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 2-Ethylacridine 207 C15H13N 1000147-64-9 9 2 6-Methyl-5-[1-piperidinyl]-2,4-p... 207 C10H17N5 1000212-53- 9 3 Corydaldine 207 C11H13NO3 000493-49-2 9 4 1,3,5-Triazine, 2-chloro-4,6-bis... 207 C5H6C1N3S2 004407-40-3 9 Abundance Scan 390 (5.371 min): 11929.D (-385) (-) m/z 207.00 0.00% 207

5000 37 _____________ j 18________________ 86 96 133 191 *I’1***I ■ • ■ ■ । ■ ■ ■ ■ । ■ 51 500 5.20 5.40 5.60 5.80 — ^tz~> 0- 4 ' i “ “ i' 10111001100010000101331’57111531111111111111711711111277 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 m/z 37.10 22.13% Abundance #84846:2-Ethylacridine 192 207 4A 5000 ■ । ■ ■ ‘ ■ । ■ ■ ■ ■ r■ • 5.00 5.20 5.40 5.60 5.80 m/z 209.00 18.14%

n/z-> 0 $2,.76,—.48+114124,140,151..4166.A78.+ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 ■p-m-

Abundance #84786:6-Methyl-5-[1-piperidinyl]-2,4-pyrimidinediamine 207

5.00 5.20 5.40 5.60 5.80 150 5000 m/z 96.00 17.14% 43 124 138 55 69 81 108 96 i, 165 178 189 ov rtp' ■ ril, ■ 11-11,Wr hhppmpo I‘‘ T miz-> ;30 40 50 60 70 80 90 100 110120130140150160 170180190 200 210 Abundance #84785: Corydaldine ■ i ■ ■ • ■ i ■ ‘ ■ i ■ ■ ■ ■ i ' 1 ■ ■ i ■ 207 5.00 5.20 5.40 5.60 5.80 m/z 132.90 16.14% 150 178 5000

163 44 53 63 7 89 104 121 135 miz—> o ------+++---4-H++4--HH lraihaas# 30 40 50 60 70 80 90 100110120130140150160 170180190 200 210 1.10792.0.1. • I ‘ ‘ ' 1 ! ‘ ‘ 5.00 5.20 5.40 ‘ • I ‘ * 1 ’ I ‘ 5.60 5.80

11929.D 052202.M Wed May 29 09:49:34 2002 Page 13

NYC-WTC_000013541

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NYC-WTC_000013541Source: NYC Law Department, mirrored locally

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