GCMS sample analysis results, AE11902, June 3, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11902.D Vial: 9 Acq On : 22 May 2002 8:20 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e 2** Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 Krypton Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T. 5.08 0.21 ug/L 135187 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Krypton 84 Kr 007439-90-9 7 2 Azetidine, 1-nitroso­ 86 C3H6N2O 015216-10-1/7 3 Thiophene 84 C4H4S 000110-02-1 5 4 Thiophene 84 C4H4S 000110-02-1 5 Abundance Scan 340 (5.077 min): 11902.D (-339) (-) m/z 84.00 100.00% 84

5000 4447 35 39 ‘ ■ 1 i * • ■ ’ i ■ ' ■ ■ i • ’ ■ ■ i ■ • ■ ■ 4.80 5.00 5.20 5.40 Oh 51 58 -HH Ppp 88 1111’1111111 “ m/z 86.00 42.84% m/z-> 15 20 25 30 35 40 45 50 55 60. 65 70 75 85 90 95 Abundance #33829: Krypton 84

5000 171/2/*/-/*"1/-/1/5/511T1/I." 4.80 5.00 5.20 5.40 42 m/z 47.05 32.97%

miz-> 15 Abundance Oh "111 “ ' 11 “ 11 “ '111 —ppmmmmmmp 20 25 30

33 35 40 45 50 55 60 65 70 . 75 #734: Azetidine, 1-nitroso- 80 80 T “ 1 ‘“ I 85 90 95 "MywARA 4.80 5.00 5.20 5.40 41 5000 86 m/z 44.00 29.60% 44 55

52 69 l 3& 0 1’1-441144 1’ —++ F8, TIPTOT fi 'i111'! IT niz-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116584: Thiophene 84 4.80 5.00 5.20 5.40 58 m/z 49.10 21.30% 45 5000 39 69 _ 50

miz—> +,+32341 Of i-rryr 15 42 ++ ,, — 1 72 -PHH 20 2530354045505560 65 70 +87 .r 1111111 ■ 111 85 90 95 75 81, 80 ■ • i ■ ■ ■ ■ i ■ ■ ■ ■ i. • ■ ■ ‘ i ‘ • 4.80 5.00 5.20 5.40

11902.D 052202.M Tue May 28 12:06:46 2002 Page 16

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