GCMS calibration data for sample AE11931, May 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\052302\11931.D vial: 11 Acq On : 23 May 2002 6:07 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L *********************************************** *•* ******************** Peak Number 8 Krypton Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

4.15 0.63 ug/L 381618 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Krypton 84 Kr 007439-90-9 9 2 Dicyandiamide 84 C2H4N4 000461-58-5/7 3 Thiophene 84 C4H4S 000110-02-1 5 4 4H-1,2,4-Triazol-4-amine 84 C2H4N4 000584-13/4 5 Abundance Scan 182 (4.149 min): 11931 .D (-180) (-) m/z 84.00 100.00% 84

Mw 5000 49

3.80 4.00 4.20 4.40 . ................ 53842.1 0- TOM—em—pn1an । > > > < j1 ■ > ■ l >i>i> * I■11■ I'»I 7 m/z 49.10 36.17% iz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33829: Krypton 84

5000 ■ ‘ i ' ‘ ■ i ■ ‘ ‘ ■ r‘ ‘ 1 1 i • ■ • ‘ i ‘ 3.80 4.00 4.20 4.40 42 m/z 86.00 31.57% 0! Mpmmpmmm]—hmm]nmmt ,1. 80 T " ■i111‘i■ m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #116556: Dicyandiamide 433 84 ■ ■ i ■ ■ ■ 1 i ■ ■ ■ ■ i ■ ■ ■ • i ■ ■ ■ ■ i ■ 3.80 4.00 4.20 4.40 5000 68 m/z 50.00 20.58%

niz-> 04TIPWTIWTTTWWTTTTTTTTTTTTI 11115358... - 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 MYMWMyhuu.k, Abundance #116585: Thiophene ■ ■ i •' ■ ■ ■ । ■ ■ ■ ■ । ' ‘ ? • i ■ ■ • ■ । ■ 84 3.80 4.00 4.20 4.40 m,z 47.10 19.95% 5000

39 45 58 /MMm. /z—> 0 ■'| | 12 | 18 42 26 32 36. ‘ ‘ . ( ■ " ■ | l I I ■ । . H I | 11 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 II111 ■ i 4l6t. 7 3.80 4.00 4.20 4.40 IT

11931.D 052202.M Wed May 29 09:50:56 2002 Page 11

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