GCMS analysis results for unknown compounds, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\060702\12739.D Vial: 15 Acq On 7 Jun 2002 7:58 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 Perdeuterobenzene Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

4.25 1.47 ug/L 1169710 1,4-dichlorobenzene-d4 9.90

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Perdeuterobenzene 84 C6D6 001076-43 2 Krypton 84 Kr 007439-90 3 Pyridine-d5- 84 C5D5N 007291-22 4 Ethyl Chloride 64 C2H5C1 000075-00 Abundance Scan 199 (4.249 min): 12739.D (-198) (-) m/z 84.00 10 84 48

5000 35 41 52 4.00 4.2b 4.40 4.60 miz- > —H+44 I 0+ " I " “ I " " I " " I ‘ ‘ ' I " " I “ 37 mmunp 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 TTp-r-rrp-rrrp-rTTp-rr-rY^^ m/z 86.00 97.41% Abundance #33650: Perdeuterobenzene 84

5000 4.00 4,20 4.40 4.60 52 56 m/z 48.05 68.60%

"Mmm.. 42 12 18 24 28, 38 48, 62 66 72 76 80 pnp Ol '' i1 ■ ■111' “ I ■1" 11 ■111111111" ■ i11111 ■ '11 “ “ I ■ ■ i '" I" ■' i1 “ ■ i' t' 11 ■ ।. 111. miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33829: Krypton 84

4.00 4.20 4.40 4.60 5000 m/z 49.10 64.63%

42 80 0l i ‘“ i" " r '" i I' ‘* I IHH — TTTTTpTnTJTTTTp-rrq- ■" i" " i • niz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33686: Pyridine-d5- 56 84 4.00 4.20 4.40 4.60 m/z 41.00 45.43% 5000 52 28 38 42 14 24 32 , 62 66 76 | 0 TIanp—Hmumtp—tt -rl-r■ ।1 > I1 ■ I,[11" । 48 ’ I 11■i■■■n■■" i■ i1 ‘" i ■1 ‘ I “111'11111 iz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.00 4.20 4.40 4.60

12739.D 060302.M Mon Jun 10 11:51:09 2002 Page 12

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