GCMS analysis results for sample AE11421, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052002\11421.D Vial: 11 Acq On : 20 May 2002 9:26 pm Operator: Mclean Sample : 5/16 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 2 Acetonitrile, dichloro­ Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

3.60 0.59 ug/L 463527 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# .al

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12/0 78 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 32 3 Allyl mercaptan 74 C3H6S 000870-23-5 9 4 lH-Pyrazole, 1-methyl- 82 C4H6N2 000930-36-9 7 Abundance Scan 89 (3.602 min): 11421 .D (-82) (-) m/ z 74.00 ’100.00% 74

82 5000 47 38 3.20 3.40 3.60 3.80 4.00 | 108 0! 1 1 1 1 1 ' 1 1 1 1 1 1 1 ' ''''n 1 ' । । J fl Ian/nnIn11’ui m/z 82.00 56.31% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

5000 82 ,104 -... r r 3.40 3.60 3.80 4.00 3.20 47 m/z 76.00 31.98% 35

miz-> Of 12 1 1 1 -1 •' r i 1 10 20 2630 1 40 Hi.... 62 . — 50 60 70 m-1 80 . 1 ■ i ‘

90 108 ■ i ' 1 ■ 1 I ■ ■ ' 1 i

100 110 Abundance #115342: Acetonitrile, dichloro- 74 35 .........hi....... 3.20 3.40 3.60 3.80 4.00 5000 82 m/z 84.00 31.83%

Of 1 1 I ' 1 1 1 1 1 1 ' 1 1 1 4 |... 47

+50— 60 ' I ' ' 1 1 I ' TIil 1 ' i ■ ■ ' ' i ' ■ 1 ■ i ■ ■ ■ ' i MWullut m/z-> 10 20 30 40 70 80 90 100 110 Abundance #28161: Allyl mercaptan 4n 74 3.20 3.40 3.60 3.80 4.00 m/z 47.05 30.12%

5000 )

47 WM/wpoasoooao ...................... . 0 |1 ' 1 1 596811 11 । 53 1 । 1 ■ 1 । 1 Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.40 3.60 3.80 4.00

11421.D 050102.M Thu May 23 10:48:25 2002 Page 5

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