GCMS analysis results, sample AE09967, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050602\9967.D Vial: 23 Acq On 7 May 2002 5:37 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Acetonitrile, dichloro- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 3.62 0.23 ug/L 172798 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-083 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 50 3 Allyl mercaptan 74 C3H6S 000870-23-5 9 4 lH-Pyrazole, 1-methyl-_______________ 82 C4H6N2 000930-36-9 7 Abundance Scan 92 (3.620 min): 9967.D (-86) (-) m/z 74.00 100.00% 74

82 5000 40 47 A y 88 3.20 3.40 3.60 3.80 4.00 1 ' । 1 1 ' 1 । ■ 1 ‘ 1 । 1 . |l . . II ! ! i’58Ia/Ii TRl 4 I । । । i । । । । । । [ i । i । r m/z 82.00 50.54% ti/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35

5000 82 11111**111* ' T1 1 1 ' I 1 ' 3.20 3.40 3.60 3.80 4.00 47 m/z 40.10 43.06% — ' i ' ' ' ' 1 1 M Tilil ' ‘ i ' ' 1 ' i ' ' ' 1 i 1 ' ' ■ i m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 7)4

1 1 1 1 1 1 1 1 1 ' I 1 1 1 1 I 1 1 ' 1 1 1 ‘ 3.20 3.40 3.60 3.80 4.00 5000 82 m/z 84.00 32.16% 47 "/ 35

m/z-> .12.... 2.000011/11 10 20 30 40 50 60 62....... 1 T1 1 1 1 1 1 70 80 , 108 I ■ i ■ ■ - ■ i ■ ■ ■ । I - - ■ ■ । 90 100 110 Abundance #28161: Allyl mercaptan 411 74 3.20 3.40 3.60 3.80 4.00 m/z 47.05 28.49% 5000

27 33 । 47 wWl WwW 1 ...... 71,37] || 53 59 , ^i.l 1 111 1 1 1 1 1 I 1 1 1 1 1 1 1 ‘ । ■ 1 । ■ ■ ■ ■ । 1 1 1 11 1 1 1 1 । /z—> 10 20 30 401 50 60 70 80 90 100 110 3.20 3.40 3.60 3.80 4.00

9967.D 050102.M Tue May 07 15:45:29 2002 Page 5

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