GCMS analysis results, sample AE09967, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050602\9967.D Vial: 23 Acq On 7 May 2002 5:37 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 2 1-Propanol, 3-chloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

3.75 0.25 ug/L 189879 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Propanol, 3-chloro- 94 C3H7C1O 000627-30-5 9 2 2-Chloroethanol 80 C2H5C1O 000107-07-3 4 3 Ethyl Chloride 64 C2H5C1 000075-00-34 4 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 2 Abundance Scan 114 (3.749 min): 9967.D (-105) (-) m/z 43.10 "100.00% 43

5000 "MyA/AWwa WAMpw 1 1 1 1 ' 1 ' 1 1 1 1 1 I ‘ 1 ' ' I 1 1 ' ' 1 1 49 59 83 88 3.40 3.60 3.80 4.00 37 11 | I I I ! | I ! I ! | I > ! I | ! I I I | I I । I | I । I > | I I I I |' I I I I | [ I I r । i i i I । i i > F] I T i T | r I । । [ I I । । | r ' I I | I । I । ' I । । | । I i । | । > I ' I" m/z 41.10 11.60% ‘[ m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #108340:1-Propanol, 3-chloro- 3h

58 5000 ‘II 3.40 3.60 3.80 4.00 41 m/z 49.10 10.17%

m/z-> 11 5 m H 111136 26 49 n 11 r ,। | । 63 11111 1111111111 68 ' । । | '~l । | 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 76 1 , i''111H " i" " i"11 r1" i " " i 93 WWhp#"yWan, Abundance #1032:2-Chloroethanol 31 ■ • i ■ । ■ ■ i ■ । । ■ i > ■ ■ ■ i ■ 3.40 3.60 3.80 4.00 5000 m/z 83.00 8.03%

15 1,1.111111111111 111 I । 1136 43 49 61 80 ' ’ l,T trrprHfi > 111 | I, , i I > n 11 n u 11 ! u I n . > I n , 11 I . i 11 n . i I m , | n .. I m'i [ /z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #107943: Ethyl Chloride n /WA ' 1 1 1 ' 1 1 i 1 1 1 1 I ‘ 1 1 1 1 1 1 ' ‘ 1 ' 23 3.40 3.60 3.80 4.00 m/z 88.00 7.90% 64 5000 y JA / 49 35 15 1 I ll i । iii i । ■ I I | 11 11 ।। i 59 TTI" --H 1 1j ii[H i11111 m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 3.40 3.60 3.80 4.00

9967.D 050102.M Tue May 07 15:45:30 2002 Page 6

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