GCMS analysis report, sample AE12763, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\l\DATA\060602\12763.D Vial: 9 Acq On 6 Jun 2002 5:49 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation .Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ******** * * *********************************************** * * ********** Peak Number 18 2-Propanone, 1,1,1-trichloro- Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T, 5.94 1.43 ug/L 1218830 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 5 2 1-Fluorononane 146 C9H19F 000463-18-3 A 3 4-Penten-2-one 84 C5H8O 013891-87-7 5 4 N-Acetylpyrrolidone 127 C6H9NO2 000932-1742 5 Abundance Scan 487 (5.941 min): 12763.D (-477) (-) m/ z 43.10 0.00% 43 __

5000

PPTTYPTPT 35 _ 125 5.60 5.80 6.00 6.20 mfe-> o+ --*PPP++ +50—61—73. + 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 97 11 11? Ii. m/z 125.00 9.75% Abundance #3877:2-Propanone, 1,1,1-trichloro- 43

5000 ■ ■ i ■ ■ 1 ■ i ■ ■ ■ ■ i ' ■ ■ ■ i

5.60 5.806.00 6.20 m/z 35.10 7.17% 15

niz-> o! HL 27 36 50—463. 76 83 97 110117125 TTtr 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 • 1 ‘ ‘ 1 ‘ l 11 ' ‘ T‘ ‘ ‘ ‘'l ' ' ' ‘ l ‘ 1 s’47 1 11 1 I ‘ ‘ 1 1 1 1 1 1 1 1 1 1 hwk Aw MM / Man MMA Abundance #4248:1-Fluorononane 43 1 1 ' 1 1 11 1 i 55 5.60 6.00 5.80 6.20 5000 29 rn/z 126.90 5.68% 70 84 97

m/z-> 15 0 TTIPTDT 10 20 136 +4 +2.+ +77l*mt 146 30 40 50 60 70 80 90 100 110 120 130 140 150 104111118126pr-rrT-yr-r-r-r-p-r 111'' 1*

Abundance #4029:4-Penten-2-one ■ ■ i ■ ■ ■ ■ i 1 ■ ■ ■ i 1 1 1 1 i ' ' 1 1 1 43 5.60 5.80 6.00 6.20 m/z 97.00 5.55% 5000

15 .. | -27 I 50 69 84 0 ' ■ I ■' ‘11 ‘ 1 ■' 11 ■ ■ ■ i •1 ■ ■ i ■ ■ ■ ■ i ■1 • ■ i " ■ ■ i ‘ ■ i ■ ■ ■ ■ i1 ■' ■ i ■ ■ ■ ■ i ■ ■' ■ i ■' ' ' i ■ ■ 1 ■ i ■ ■ • ■ i ' 1 1 ' I 1 1 1 1 I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 5.60 5.80 6.00 6.20

12763.D 060302.M Mon Jun 10 10:29:11 2002 Page 21

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