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GCMS analysis report, sample AE12763, June 2002

Machine-extracted title · confidence 95%

Gas chromatography-mass spectrometry results for sample AE12763 analyzed on June 12, 2002.

NYC-WTC_000015777–000015805

Folder label: “GCMS X 6/11/02 A 6/11/02

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NYC 9/11 Public Portal Document Library searen compound. Report

Data File C:\MSDCHEM\1\DATA\060602\12763.D Vial: 9 Acq On 6 Jun 2002 5:49 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L Peak Number 19 Anthracene-dlO- Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.39 ug/L 503637 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-diO- 188 C14D10 001719-06-8 47' 2 1,4-Naphthoquinone, 2,3-dihydro-... 188 C12H1202 1000157-22-3 42 3 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 38 4 Phenanthrene-diO 188 C14D10 001517-22-2 37 Abundance Scan 3401 (23.062 min): 12763.D (-3395) (-) m/z 188.10 100.00% US

5000

80 94 160 1 23.00 22.80 23.20 23.40 43 57 66 A-H-T n/z-> 0 mTTTTTTTTPTT --HH+ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 11 m/z 189.10 19.42% Abundance #79826: Anthracene-d10- US

5000 22.80 23.00 23.20 23.40 m/z 184.10 17.29% 80 94 160 , , 17 30 42 52 66 108118 132 ,146, 11179179.1. O- TPWWITTTTTTTTTT-HH 111' “11 “1' i1 ■ “ I" " miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79805:1,4-Naphthoquinone, 2,3-dihydro-5,8-dimethyl- US -------------------- 173 22.80 23.00 23.20 23.40 5000 145 m/z 94.05 15.76% 82 91 159 27 39 51 65 । 105 115 131 0 44444, Tir tumn miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79714: Pentacyclo[8.4.0.0(3,7).0(4,14).0(6,11 )tetradecane US 8......... 22.80 23.00 23.20 23.40 • m/z 160.00 10.73%

5000 79 91 106 117 131 145 159 173

m/z—> 0- 27—11557h y 4 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

12763.D 060302.M Mon Jun 10 10:29:12 2002 Page 22

NYC-WTC_000015803

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NYC-WTC_000015803Source: NYC Law Department, mirrored locally

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