GCMS sample AE12765 results, June 6 2002

NYC 9/11 Public Portal Document Library Searen Compound Report Data File C: \MSDCHEM\ 1 \DATA\06040212765.D Vial: 6 Acq On 4 Jun 2002 7:55 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L Peak Number 16 Anthracene-dlO- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.28 ug/L 267305 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 87 ) 2 Phenanthrene-diO 188 C14D10 001517-22-2 87 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 38 Abundance Scan 3401 (23.062 min): 12765.D (-3395) (-) m/z 188.10 100.00% 188

5000 80 - 66 94 160 . , 22.80 23.00 23.20 23.40

tt/z-> 49 0 ' i ■ “ ■ i “ “ i • • ■ ■ i •1 ■ ‘"i" 132 ---HTDWTTTLWTTTTTTTTTTTTTTT 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 4 m/ z 80.10 19.59% Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 189.20 15.12% 17 30 42 52 66। . 80 , 108118 132 146 1I.16094 170179. ,| 0 ■ i' • ••i ‘ l' “111111111' TTTTTHTTTTTTNTTTTTTTTTTT ‘T miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 184.10 13.82%

80 94 160 30 42 52 66 . 11 108118 132 146 I. 170179,,I 0 1W0pp——apHpm 1hepmpo"T miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline .. t ....... ....... 188 22.80 23.00 23.20 23.40 m/ z 94.05 12.37% 145 5000

41 51 63 77 89 102 117 130 159 173 O-Mm T+H— tt- Tyrrt 11911 n/z—> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

12765.D 060302.M Wed Jun 05 14:05:49 2002 Page 19

NYC-WTC_000015559