GCMS sample AE12765 results, June 6 2002

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Gas chromatography-mass spectrometry analysis report for sample AE12765 detecting unknown compounds and surrogates on June 6, 2002.

NYC-WTC_000015536–000015560

Folder label: “GCMS X 6/4/02 A 6/4/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\060402\12765.D Vial: 6 Acq On 4 Jun 2002 7:55 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 15 Anthracene, 2-methyl- Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 22.53 0.25 ug/L 237406 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 53 2 Anthracene, 9-methyl- 192 C15H12 000779-02-2 53 3 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 53 4 Anthracene, 9-methyl- 192 C15H12 000779-02-2 53 Abundance Scan 3311 (22.533 min): 12765.D (-3303) (-) m/z 192.10 100.00% 192

5000 - 82 96 146 1 Rn . 22.20 22.40 22.60 22.80 0 40 52 70 7 J | 160 J], m/z 191.10 16.42% iz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #1 25844: Anthracene, 2-methyl- 1912

- 5000 TTI 22.20 22.40 22.60 22.80 m/z 193.10 15.18% 96 165 63 74 83 115 1139 150 I 176 0 ■ i “ “ i" " i1 “11" " i■ iiri 11’"1 ■' mmmnmmphpt ^TT

miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125848: Anthracene, 9-methyl- 192

22.20 22.40 22.60 22.80 5000 m/Z 96.10 14.41%

96 P 27 39 51 63 .82 l 115 126 139 152 ,,176 „| o1 11 i m । n 11‘| i 111 |*i 1111i*m1 Ttfi pifi f!‘| r’l’l 11 111 i pri 11 m m । m ip| mt ph 111 t’t’t 11 i rh 111 MI‘‘1 i । 11 । n/z-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance» #125856: Phenanthrene, 1-methyl- 192 22.20 22.40 22.60 22.80 m/z 146.10 13.54% A 5000

/z—> 27 39 51 63 0 ■ i ■ ■' ■ i “ " i" ■ ■ i" " i ■ i 82 ,11 96 115 126 139 152 190 178 = - 1 111! ■ । ■ u i |-i ri 111 > 111, । irp > 11 |’l i i 11 i’t’t 17 i rlh । । i‘lJ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 u A 22.20 22.40 22.60 22.80 i

12765.D 060302.M Wed Jun 05 14:05:48 2002 Page 18

NYC-WTC_000015558

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