GCMS analysis results for sample AE11930, June 2002

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Laboratory report documenting GCMS analysis of sample AE11930 conducted on June 4, 2002.

NYC-WTC_000013551–000013573

Folder label: “GCMS X 5/22/02 A 5/23/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\11930.D Vial: 10 Acq On : 23 May 2002 5:18 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 12 Anthracene, 9-methyl- Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 22.54 0.26 ug/L 231618 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene, 9-methyl- 192 C15H12 000779-02-2 42 2 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5/42 3 Anthracene, 2-methyl- 192 C15H12 000613-12-7 42 4 Anthracene, 9-methyl- 192 C15H12 000779-02/2 42 Abundance Scan 3312 (22.539 min): 11930.D (-3302) (-) m/z 192.10 100.00% 192

5000 11 22.20 22.40 22.60 22.80

m/z-> 0 .. 14.... .......... 118.... X..T..... ,i 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 m/z 193.10 17.92% Abundance #125848: Anthracene, 9-methyl- 192

5000 1' । ■ • ■ ■ । ■ • ■ ■ । ■ ■ ■ • । ■ ■ ■ ■ । 22.20 22.40 22.60 22.80 m/z 191.00 15.67% 27 39 51 63 82 961 ace 115 126 139 152 । 176 „ 0- !. . . . ,.. . ■ fl , . i । !'i ■ > | ■ "plth m i । r. i > | i i'i 1 । 1 i l l | i > > i'| i i I I |'l 1 11 | I'l'l i । 11 I i | i 11'1' TT n/z-> 2030405060 70 8090 100 110 120 130140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

22.20 22.40 22.60 22.80 5000 m/z 146.10 14.25%

29 39 51 63 74 83 115 126 139 152 165 176 | 0 TDWTTTPTgmmmmTTt "Ti mfz~> 20 30 40 50 60 70 80 90 100 110 120 130140 150 160 170 180 190 200 Abundance #125844: Anthracene, 2-methyl- । । । i । A । । । 11 -j-i -i । -i । 192 22.20 22.40 22.60 22.80 m/z 96.00 11.49% 5000

96 165 63 74 25 ,|| 115 139 150 176 0- I “ " I''1' I “ “ I‘ I • r'' h 11'111111 111 ri 11 111111111'| i > > i |t m ] 11 i । ■ I 1111 i’1 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22 60 22.80

11930.D 052202.M Wed May 29 09:50:19 2002 Page 15

NYC-WTC_000013570

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NYC-WTC_000013570Source: NYC Law Department, mirrored locally

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NYC-WTC_000013476

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