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GCMS analysis results for sample AE11381, May 22 2002

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Laboratory report showing GCMS analysis results for sample AE11381 conducted on May 22, 2002.

NYC-WTC_000025102–000025126

Folder label: “GCMS X 5/15/02 A 5/17/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\051702\11380.D Vial: 7 Acq On : 17 May 2002 5:40 pm Operator: Mclean Sample : 5/15 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 Anthracene, 2-methyl- Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 22.58 0.31 ug/L 387264 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 64 2 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 3 Bitoscanate 192 C8H4N2S2 004044-65-9 53 4 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 50 Abundance Scan 3319 (22.580 min): 11380. D (-3309) (-) m/z 192.10 100.00% 192 I 5000

42 52 70 82 %6 120 146 160 11 4 I'' . 11" 11 .... n... a. 22.20 22.40 22.60 22.80 23.00

m/z-> 0 ■ > । ■ i I I J I । iT H' i i । i । I i j i । I I |~r4 I I । i J I । । i i r i y i i i I | I । । । । i

20 30 40 50 60 70 80 90 100110120130140150 160170180190 200 210 .. 11.297 m/z 191.10 23.66% Abundance #125845: Anthracene, 2-methyl- 192

- 5000 22.20 22.40 22.60 22.80 23.00 m/z 193.00 15.61% 66 75 87 96 115 126 139 152 165 1/6 0 । | । । i •] । । ri | i । i i i i ] i i i 1 । i Mlrrli l'P| i Pl 1'|'i i i । ।' i'i'i । [ । 11 i 11 । i I1] r t t t ^'| i i i । I rt TTTTt’h i i i'l .....1 m/z-> 20 30 40 50 60 70 80 90 100 110120130140150 160 170180190 200 210 Abundance #81033: Phenanthrene, 9-methyl- 192 1 I ' ' ' ' I ' 1 ‘‘I 111 22.20 22.40 22.60 22.80 23.00 5000 m/z 146.10 14.15%

96 165 i । 29 39 51 63 74 83 J 115 126 139 152 j 1/6 . | 0 11" " r ‘" i' " ■ I'1" i" rri 11'' i'111 r ■1111 ri' 11111 r '1 ''11'111'1" 111’l’l' I' r’ll 111 "‘Il " i" " ।1" m/z-> 20 30 40 50 60 70 80 90 100 110120130140150160170180 190 200 210 Abundance #125828: Bitoscanate ----------- 192 22.20 22.40 22.60 22.80 23.00 m/z 96.00 11.79%

5000

134 90 160 50 63 75

m/z-> 0 -4+ —H, ,102 122 l'l rl'p'lTi j " ih i 1111 [■! 11 1111

20 30 40 50 60 70 80 90 100110120 130 140 150 160170 180 190 200 210 148 176 ‘"I"1'..... 'I'"1 11"1' i" " i p-rr ! 1 1 1 1 1 I ' 1 1 ' r' ' ' 1 1 1 1 22.20 22.40 22.60 22.80 23.00 TIm

11380.D 050102.M Mon May 20 15:46:52 2002 Page 10

NYC-WTC_000025119

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NYC-WTC_000025119Source: NYC Law Department, mirrored locally

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