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GCMS analysis results for sample AE11381, May 22 2002

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Laboratory report showing GCMS analysis results for sample AE11381 conducted on May 22, 2002.

NYC-WTC_000025102–000025126

Folder label: “GCMS X 5/15/02 A 5/17/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\051702\11380.D Vial: 7 Acq On : 17 May 2002 5:40 pm Operator: Mclean Sample : 5/15 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Cyclopentasiloxane, decamet... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 12.41 0.73 ug/L 884318 Napthalene-d8 13.43

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H30O5S15 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H30O5S15 000541-02-6 38 3 Phenethylamine, N-methyl-.beta. ,... 399 C18H37NO3Si3 010538-85-9 38 4 Benzeneethanamine, N-[(pentafluo... 475 C21H26F5NO2Si2 055429-85-1 28 Abundance Scan 1588 (12.410 min): 11380.D (-1580) (-) m/z 73.10 100.00% 73

5000

45 267 355 m 12.00 12.20 12.40 12.60 12.80

m/z-> 0 । i L 108 133 154170, 193 , 223 249 — 323 ■ p " ‘ r ■' 'i1 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 r7 1 m/ z 2 67.00 41.01% Abundance #115273: Cyclopentasiloxane, decamethyl- 73

5000 267 12.00 12.20 12.40 12.60 12.80 355 m/z 355.00 30.97% 45 0- 28 .... . ............. 193 223 249 96 115133 165 .. .. 1 ■ ।1 * * * ।1 <1 'I ■ ‘141 ‘ 4 1**2 293 323 n/z- > :20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #115315: Cyclopentasiloxane, decamethyl- 73 ........ ............. 355 12.00 12.20 12.40 12.60 12.80 267 5000 m/ z 356.00 11.50%

45 323 I 0 11111' 11" —2729mH I' "' 11 " 111" 11'11' 111111'11' 1 “ 1' ]1''11" " I'111111111'1 1111 ’!'1' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #115313: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... |....... . 73 12,00 12.20 12.40 12.60 12.80 m/ z 2 68.00 11.00%

5000 355

44 . , 93 130147 193 220237 384 267 294 | 0 V7 , , , |TTif71 ITI 11।, 11 ilia 1TT fi n i -p i r i p -i 11 [i 11111111 p-’t 11 p i i'r p ri i p i! i p 11") i 11 T-p-r-r mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 12.00 12.20 12.40 12.60 12.80

11380.D 050102.M Mon May 20 15:46:50 2002 Page 9

NYC-WTC_000025118

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NYC-WTC_000025118Source: NYC Law Department, mirrored locally

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