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GCMS sample analysis results, AE11904, June 3, 2002

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Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11904.

NYC-WTC_000012937–000012965

Folder label: “GCMS X 5-21-02 A 5-22-02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11904.D Vial: 11 Acq On : 22 May 2002 9:58 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan 1* Library- : C:\DATABASE\NIST98.L ************************************************************** * * ***** Peak Number 13 Cyclopentasiloxane, decamet... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 12.38 0.88 ug/L 849409 Napthalene-d8 13.39 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 3 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 4 Benzeneethanamine, N-[(pentafluo... 563 C24H34F5NO3Si3 055429-13-5 43 Abundance Scan 1582 (12.374 min): 11904.D (-1575) (-) m/z 73.10 100.00%! 73

5000 267 355 m 45 12.00 12.20 12.40 12.60 12.80 119 154 193 223 249 1 323 . t 0- TI—TugmT’T ■ 11" " i' “ 'I ■ ■ ■ fi" i ■ “ m/z 267.00 38.04%| niz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #115315: Cyclopentasiloxane, decamethyl- 73

355 267 5000 12.00 12.20 12.40 12.60 12.80 m/z 355.10 29.16 45 _____________________________ 207 323 249 0 ■I l.... I I I.. ."I mpmm TTBg—T 111 > 111111TTTI 111111! I ! | rt I > 111 > 111 11 r n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 3(X) 320 340 360 380 Abundance #115273: Cyclopentasiloxane, decamethyl- 73 1 12.00 12.20 12.40 12.60 12.80 5000 267 m/z 268.00 11.63%| 355 45 28.1. 96 115133 165,193 2233 249 { 293 323 0- 11111' |>1 "T" n | >'TI—mupugTu!WTTmmt- n/z-> 20 40 60 80 100 120 140 160180 200 220 240 260 280 300 320 340 360 380 Abundance #115313: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... ■ i ■ ‘ ‘ ■ i ■ ■ -r-r-j-n-r-ry-r 73 12.00 12.20 12.40 1260 1280 m/z 356.00 8.03%|

5000 355 44

0 -HIThupuMmpg , 93 130147 193 220237 267 294 i 384 TUWT"ug—r ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i * * • ' । * /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 12.00 12.20 12.40 12.60 12.80

11904.D 052202.M Tue May 28 12:09:22 2002 Page 16

NYC-WTC_000012957

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NYC-WTC_000012957Source: NYC Law Department, mirrored locally

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