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GCMS sample analysis results, AE11903, June 3, 2002

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Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.

NYC-WTC_000012908–000012936

Folder label: “GCMS X 5-21-02 A 5-22-02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11903.D Vial: 10 Acq On : 22 May 2002 9:09 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library . : C:\DATABASE\NIST98.L ****************** ** ************************ * * *********************** Peak Number 11 Cyclopentasiloxane, decamet... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 12.38 1.26 ug/L 1256140 Napthalene-d8 13.40 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6/58 3 N-(Trifluoracetyl)-0,0',O'’-tris... 495 C20H36F3NO4Si3 054135-51-2 43 4 Benzeneethanamine, N-[ (pentafluo. . . 563 C24H34F5NO3Si3 055429-13-5 37 Abundance Scan 1582 (12.374 min): 11903.D (-1576) (-) m/z 73.10 00.00% 73

5000 267 355 12.00 12.20 12.40 12.60 12.80 45 0- —r4 1 125 154 193.223 .4., 1 323 I 1 1 • 1 • ■ i ■ • ■ ■ i 1 m/z 267.00 37.49% miz—> 50 100 150 200 250 300 350 400 450 500 Abundance #115315: Cyclopentasiloxane, decamethyl- 73

355 267 ............. / t .............. 5000 12.00 12.20 12.40 12.60 12.80 m/z 355.10 26.70% 45 207 I 323 Qi —-'i । i , I , . -rI51IO — I slat . BE/UKBTI8 L - ■ ■ i ‘ ' 1 i ' ■ • ■ i ■ miz-> 50 100 150 200 250 300 350 400 450 500 Abundance #115273: Cyclopentasiloxane, decamethyl- 73

12.00 12.20 12.40 12.60 12.80 5000 267 m/z 356.10 10.90% 355 45 0 . .1 1 ‘ 1 i ' 96 > > ' i ■ 133 165.193223, 1 ;293 3231.............. n/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #27963: N-(Trifluoracetyl)-O,O',O“-tris(trimethyteiIyl)ep... ■ i • • ■ • t ' ■ ‘ ■ i ' 1 1 ■ i ■ 73 12.00 12.20 12.40 12.60 12.80 355 m/z 268.00 9.94% 5000

45

miz—> 0 r , 1, yh ,. 110 51?. 184207.251.281 3241 11*1* 480 • i ■ • ■ • i • • 1 1 1 ' ' 1 1 I 1 50 100 150 200 250 300 350 400 450 500 12.00 12.20 12.40 12.60 12.80

11903.D 052202.M Tue May 28 12:07:50 2002 Page 14

NYC-WTC_000012926

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NYC-WTC_000012926Source: NYC Law Department, mirrored locally

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