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GCMS sample analysis results, AE11907, June 4, 2002

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Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.

NYC-WTC_000012989–000013013

Folder label: “GCMS X 5-21-02 A 5-22-02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11907.D Vial: 14 Acq On : 23 May 2002 12:25 am Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan 71 Library- : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 11 Cyclopentasiloxane, decamet... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 12.37 1.36 ug/L 1063780 Napthalene-d8 13.39 Hit# of 5 Tentative ID MW MolForm CAS# Qu. 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6(90 2 Cyclopentasiloxane, decamethyl- 370 C10H3005S15 000541-02-6 53 3 Benzeneethanamine, N- (pentafluo... 475 C21H26F5NO2Si2 055429-85-1 38 4 Benzeneethanamine, N- (pentafluo... 563 C24H34F5NO3Si3 055429-13-5 35 Abundance Scan 1582 (12.374 min): 11907.D (-1573) (-) m/z 73.10 100.00% 73

5000 267 355

45 12.00 12.20 12.40 12.60 12.80

iz-> 1 ,103 -223.411-2394 133 154 177193 04pnnnTTTTTTTTTTp-TTTYTTTTpTTTyrTrr^^ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 m/z 267.00 40.14% Abundance #115273: Cyclopentasiloxane, decamethyl- 73

5000. 267 TT ’I T ‘IiT 12.00 12.20 12.40 12.60 12.80 355 m/Z 355.10 29.13% 45

miz-> 28 0-— J ++49,115,133149165.193234M. i 307323339 TIpmm L 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 . Abundance #115315: Cyclopentasiloxane, decamethyl- 73

355 12.00 12.20 12.40 12.60 12.80 267 m/z 268.00 10.74% 5000

45 niz-> 191207223 251 1... 111132337%, 0- 1... H 1 . j.. r. r ... |i 1111 j 111 p u i j 111 j j. i V11 m it 11 j 111 , j 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 T’’ Abundance #115266: Benzeneethanamine, N-Kpentafluorophenyl)methylen... .in 73 12 00 12.20 12.40 12.60 12.80 m/z 356.10 10.52% 5000 267 44 , 91 117135151 179 209 250 .................. oW .. f. ’“u—mB——uddm——ou—Bhp*deoh*a—hodgorm— i-i r[ rf-i 1111 i riri ri| 111111.1111, TI’4I-’4* ■ ‘ i ' ■ ■ ■ i ■ n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12.00 12.20 12.40 1260 12.80

11907.D 052202.M Tue May 28 12:14:30 2002 Page 14

NYC-WTC_000013007

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NYC-WTC_000013007Source: NYC Law Department, mirrored locally

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